3-Benzoyl-benzoic acid (E)-4-(2-chloro-acetoxy)-2-methyl-but-2-enyl ester

Base Information

Chemical Name:3-Benzoyl-benzoic acid (E)-4-(2-chloro-acetoxy)-2-methyl-but-2-enyl ester
CAS No.:180045-88-9
Molecular Formula:C₂₁H₁₉ClO₅
Molecular Weight:386.832
Hs Code.:

Synonyms:3-Benzoyl-benzoic acid (E)-4-(2-chloro-acetoxy)-2-methyl-but-2-enyl ester

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Chemical Property of 3-Benzoyl-benzoic acid (E)-4-(2-chloro-acetoxy)-2-methyl-but-2-enyl ester

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Technology Process of 3-Benzoyl-benzoic acid (E)-4-(2-chloro-acetoxy)-2-methyl-but-2-enyl ester

There total 3 articles about 3-Benzoyl-benzoic acid (E)-4-(2-chloro-acetoxy)-2-methyl-but-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 77301-47-4
3-benzoylbenzoyl chloride

: 88887-92-7
(E)-3-Methyl-l-chloroacetoxy-2-buten-4-ol

: 180045-88-9
3-Benzoyl-benzoic acid (E)-4-(2-chloro-acetoxy)-2-methyl-but-2-enyl ester

Guidance literature:: In pyridine;
DOI:10.1016/0040-4039(96)00972-0

Reference yield:

: 556-82-1
3-methyl-2-buten-1-ol

: 180045-88-9
3-Benzoyl-benzoic acid (E)-4-(2-chloro-acetoxy)-2-methyl-but-2-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine, DMAP / CH₂Cl₂

2: t-BuOOH, H₂SeO₃, salicylic acid / CH₂Cl₂

3: 57 percent / pyridine

With pyridine; tert.-butylhydroperoxide; dmap; selenious acid; salicylic acid; In pyridine; dichloromethane;
DOI:10.1016/0040-4039(96)00972-0

Reference yield:

: 88887-91-6
Chloro-acetic acid 3-methyl-but-2-enyl ester

: 180045-88-9
3-Benzoyl-benzoic acid (E)-4-(2-chloro-acetoxy)-2-methyl-but-2-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOOH, H₂SeO₃, salicylic acid / CH₂Cl₂

2: 57 percent / pyridine

With tert.-butylhydroperoxide; selenious acid; salicylic acid; In pyridine; dichloromethane;
DOI:10.1016/0040-4039(96)00972-0