4-(4-chloro-3-ethylphenoxy)-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-5-yl)benzaldehyde

Base Information

Chemical Name:4-(4-chloro-3-ethylphenoxy)-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-5-yl)benzaldehyde
CAS No.:1355656-59-5
Molecular Formula:C₂₃H₂₃ClN₂O₃
Molecular Weight:410.9
Hs Code.:

Synonyms:4-(4-chloro-3-ethylphenoxy)-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-5-yl)benzaldehyde

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Chemical Property of 4-(4-chloro-3-ethylphenoxy)-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-5-yl)benzaldehyde

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Technology Process of 4-(4-chloro-3-ethylphenoxy)-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-5-yl)benzaldehyde

There total 3 articles about 4-(4-chloro-3-ethylphenoxy)-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-5-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 903550-26-5
1-tetrahydropyran-1H-pyrazolylboronic ester

: 1355656-57-3
3-bromo-4-(4-chloro-3-ethylphenoxy)benzaldehyde

: 1355656-59-5
4-(4-chloro-3-ethylphenoxy)-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-5-yl)benzaldehyde

Guidance literature:: With caesium carbonate; In 1,4-dioxane; water; at 75 ℃; for 18h; Inert atmosphere;

Reference yield:

: 14143-32-9
4-chloro-3-ethylphenol

: 1355656-59-5
4-(4-chloro-3-ethylphenoxy)-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-5-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / dimethyl sulfoxide / 0.02 h

1.2: 5 h / 50 °C

2.1: caesium carbonate / 1,4-dioxane; water / 18 h / 75 °C / Inert atmosphere

With potassium carbonate; caesium carbonate; In 1,4-dioxane; water; dimethyl sulfoxide;

Reference yield:

: 77771-02-9
3-bromo-4-fluorobenzaldehyde

: 1355656-59-5
4-(4-chloro-3-ethylphenoxy)-3-(1-(tetrahydro-2H-pyran-2-yl)-1H-pyrazol-5-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / dimethyl sulfoxide / 0.02 h

1.2: 5 h / 50 °C

2.1: caesium carbonate / 1,4-dioxane; water / 18 h / 75 °C / Inert atmosphere

With potassium carbonate; caesium carbonate; In 1,4-dioxane; water; dimethyl sulfoxide;