1(2H)-Naphthalenone,3,4-dihydro-6-methoxy-2-methyl-2-(2-propenyl)-,(2S)-(9CI)

Base Information

Chemical Name:1(2H)-Naphthalenone,3,4-dihydro-6-methoxy-2-methyl-2-(2-propenyl)-,(2S)-(9CI)
CAS No.:812639-16-0
Molecular Formula:C₁₅H₁₈O₂
Molecular Weight:230.307
Hs Code.:
Mol file:812639-16-0.mol

Synonyms:1(2H)-Naphthalenone,3,4-dihydro-6-methoxy-2-methyl-2-(2-propenyl)-, (2S)- (9CI)

Suppliers and Price of 1(2H)-Naphthalenone,3,4-dihydro-6-methoxy-2-methyl-2-(2-propenyl)-,(2S)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 1(2H)-Naphthalenone,3,4-dihydro-6-methoxy-2-methyl-2-(2-propenyl)-,(2S)-(9CI)

Chemical Property:

PSA：26.30000
LogP:3.40650

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1(2H)-Naphthalenone,3,4-dihydro-6-methoxy-2-methyl-2-(2-propenyl)-,(2S)-(9CI)

There total 7 articles about 1(2H)-Naphthalenone,3,4-dihydro-6-methoxy-2-methyl-2-(2-propenyl)-,(2S)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 812639-04-6
allyl 6-methoxy-2-methyl-3,4-dihydronaphthalen-1-yl carbonate

: 812639-16-0
2-allyl-6-methoxy-2-methyl-1-tetralone

Guidance literature:: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; In tetrahydrofuran; at 10 ℃; for 8h; Product distribution / selectivity;

Reference yield:

: 591-87-7
Allyl acetate

: 27752-24-5,888007-82-7,1129429-21-5,745033-23-2
6-methoxy-2-methyl-3,4-dihydronaphthalen-1(2H)-one

: 812639-16-0
2-allyl-6-methoxy-2-methyl-1-tetralone

: 812639-16-0
2-allyl-6-methoxy-2-methyl-1-tetralone

Guidance literature:: With trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); bis(η3-allyl-μ-chloropalladium(II)); trimethyltin(IV)chloride; lithium diisopropyl amide; In 1,2-dimethoxyethane; for 1h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/ja991135b

Reference yield:

: 591-87-7
Allyl acetate

: 27752-24-5,888007-82-7,1129429-21-5,745033-23-2
6-methoxy-2-methyl-3,4-dihydronaphthalen-1(2H)-one

: 812639-16-0
2-allyl-6-methoxy-2-methyl-1-tetralone

: 812639-16-0
2-allyl-6-methoxy-2-methyl-1-tetralone

Guidance literature:: With trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); bis(η3-allyl-μ-chloropalladium(II)); trimethyltin(IV)chloride; lithium diisopropyl amide; In 1,2-dimethoxyethane; for 1h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/ja991135b