N-{2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]ethyl}-N'-phenyloxalamide

Base Information

Chemical Name:N-{2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]ethyl}-N'-phenyloxalamide
CAS No.:306968-21-8
Molecular Formula:C₂₄H₂₉N₃O₄
Molecular Weight:423.512
Hs Code.:

Synonyms:N-{2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]ethyl}-N'-phenyloxalamide

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Chemical Property of N-{2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]ethyl}-N'-phenyloxalamide

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Technology Process of N-{2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]ethyl}-N'-phenyloxalamide

There total 4 articles about N-{2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]ethyl}-N'-phenyloxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1457-85-8
Ethyl oxanilate

: 194612-31-2
2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]-2-ethylamine

: 306968-21-8
N-{2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]ethyl}-N'-phenyloxalamide

Guidance literature:: In ethanol; for 3h; Heating;
DOI:10.1021/jm991121g

Reference yield:

: 1094-91-3
2-(toluene-4-sulfonyloxymethyl)-2,3-dihydro-benzo[1,4]dioxine

: 306968-21-8
N-{2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]ethyl}-N'-phenyloxalamide

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / 20 h / 140 °C

2: 95 percent / LiAlH₄ / tetrahydrofuran / Heating

3: 48 percent / ethanol / 3 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; ethanol; 1: Alkylation / 2: Reduction / 3: Condensation;
DOI:10.1021/jm991121g

Reference yield:

: 78056-67-4
1-(phenylmethyl)-4-piperidineacetonitrile

: 306968-21-8
N-{2-[1-(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)piperidin-4-yl]ethyl}-N'-phenyloxalamide

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / 20 h / 140 °C

2: 95 percent / LiAlH₄ / tetrahydrofuran / Heating

3: 48 percent / ethanol / 3 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; ethanol; 1: Alkylation / 2: Reduction / 3: Condensation;
DOI:10.1021/jm991121g