(Benzyloxycarbonylamino)thioacetimidsaeure-methylester-fluorsulfonat

Base Information

Chemical Name:(Benzyloxycarbonylamino)thioacetimidsaeure-methylester-fluorsulfonat
CAS No.:140903-32-8
Molecular Formula:C₁₁H₁₄N₂O₂S*FHO₃S
Molecular Weight:338.381
Hs Code.:

Synonyms:(Benzyloxycarbonylamino)thioacetimidsaeure-methylester-fluorsulfonat

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Chemical Property of (Benzyloxycarbonylamino)thioacetimidsaeure-methylester-fluorsulfonat

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Technology Process of (Benzyloxycarbonylamino)thioacetimidsaeure-methylester-fluorsulfonat

There total 2 articles about (Benzyloxycarbonylamino)thioacetimidsaeure-methylester-fluorsulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 421-20-5
Methyl fluorosulfonate

: 49548-40-5
N-benzyloxycarbonylglycine thioamide

: 140903-32-8
(Benzyloxycarbonylamino)thioacetimidsaeure-methylester-fluorsulfonat

Guidance literature:: In dichloromethane; for 2.5h; Ambient temperature;

Reference yield:

: 3589-41-1
phenylmethyl cyanomethylcarbamate

: 140903-32-8
(Benzyloxycarbonylamino)thioacetimidsaeure-methylester-fluorsulfonat

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / gaseous H₂S, Na₂S*10H₂O, tricaprylmethylammonium chloride / H₂O; benzene / 6 h / 70 °C

2: 93 percent / CH₂Cl₂ / 2.5 h / Ambient temperature

With sodium sulfide; hydrogen sulfide; Aliquat 336; In dichloromethane; water; benzene;