2,5-dihydro-4-methyl-5-<(1,3-dimethyl-2-oxocyclohexyl)methyl>-2-oxo-3-furancarboxylic acid methyl ester

Base Information

Chemical Name:2,5-dihydro-4-methyl-5-<(1,3-dimethyl-2-oxocyclohexyl)methyl>-2-oxo-3-furancarboxylic acid methyl ester
CAS No.:74063-87-9
Molecular Formula:C₁₆H₂₂O₅
Molecular Weight:294.348
Hs Code.:

Synonyms:2,5-dihydro-4-methyl-5-<(1,3-dimethyl-2-oxocyclohexyl)methyl>-2-oxo-3-furancarboxylic acid methyl ester

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Chemical Property of 2,5-dihydro-4-methyl-5-<(1,3-dimethyl-2-oxocyclohexyl)methyl>-2-oxo-3-furancarboxylic acid methyl ester

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Technology Process of 2,5-dihydro-4-methyl-5-<(1,3-dimethyl-2-oxocyclohexyl)methyl>-2-oxo-3-furancarboxylic acid methyl ester

There total 4 articles about 2,5-dihydro-4-methyl-5-<(1,3-dimethyl-2-oxocyclohexyl)methyl>-2-oxo-3-furancarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 60971-99-5
2,5-dihydro-4-methyl-5-methylene-2-oxo-3-furancarboxylic acid methyl ester

: 63547-53-5
2,6-dimethyl-1-(trimethylsiloxy)cyclohexene

: 74063-87-9
2,5-dihydro-4-methyl-5-<(1,3-dimethyl-2-oxocyclohexyl)methyl>-2-oxo-3-furancarboxylic acid methyl ester

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -78 ℃;
DOI:10.1021/ja00527a046

Reference yield:

: 60971-98-4
2,5-dihydro-5-hydroxy-4,5-dimethyl-2-oxo-3-furancarboxylic acid methyl ester

: 74063-87-9
2,5-dihydro-4-methyl-5-<(1,3-dimethyl-2-oxocyclohexyl)methyl>-2-oxo-3-furancarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / phosphorus pentoxide, methanesulphonic acid / 1.5 h / Ambient temperature

2: 32 percent / titanium tetrachloride / CH₂Cl₂ / -78 °C

With phosphorus pentaoxide; methanesulfonic acid; titanium tetrachloride; In dichloromethane;
DOI:10.1021/ja00527a046

Reference yield:

: 60971-97-3
2,5-dihydro-5-hydroxy-4,5-dimethyl-2-oxo-3-furancarboxylic acid

: 74063-87-9
2,5-dihydro-4-methyl-5-<(1,3-dimethyl-2-oxocyclohexyl)methyl>-2-oxo-3-furancarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / diethyl ether

2: 95 percent / phosphorus pentoxide, methanesulphonic acid / 1.5 h / Ambient temperature

3: 32 percent / titanium tetrachloride / CH₂Cl₂ / -78 °C

With phosphorus pentaoxide; methanesulfonic acid; titanium tetrachloride; In diethyl ether; dichloromethane;
DOI:10.1021/ja00527a046