4-methylene-2-phenyl-5-oxo-4,5-dihydro-1,3-oxazole

Base Information

Chemical Name:4-methylene-2-phenyl-5-oxo-4,5-dihydro-1,3-oxazole
CAS No.:3161-47-5
Molecular Formula:C₁₂H₁₁NO₂S₂
Molecular Weight:265.357
Hs Code.:

4-<bis(methylthio)>methylene-2-phenyl-5-oxo-4,5-dihydro-1,3-oxazole

Synonyms:4-methylene-2-phenyl-5-oxo-4,5-dihydro-1,3-oxazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methylene-2-phenyl-5-oxo-4,5-dihydro-1,3-oxazole

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Technology Process of 4-methylene-2-phenyl-5-oxo-4,5-dihydro-1,3-oxazole

There total 6 articles about 4-methylene-2-phenyl-5-oxo-4,5-dihydro-1,3-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2
Hippuric Acid

: 75-15-0,12122-00-8
carbon disulfide

: 77-78-1
dimethyl sulfate

: 3161-47-5
4-methylene-2-phenyl-5-oxo-4,5-dihydro-1,3-oxazole

Guidance literature:: Hippuric Acid; With chloroformic acid ethyl ester; triethylamine; In benzene; for 0.5h; Inert atmosphere;

carbon disulfide; With triethylamine; In benzene; Inert atmosphere;

dimethyl sulfate; In benzene; at 0 ℃; Inert atmosphere;
DOI:10.1021/jo100941f