1,1-bis[dimethylamino(phenyl)boryl]methane

Base Information

Chemical Name:1,1-bis[dimethylamino(phenyl)boryl]methane
CAS No.:1356370-15-4
Molecular Formula:C₁₇H₂₄B₂N₂
Molecular Weight:278.013
Hs Code.:

Synonyms:1,1-bis[dimethylamino(phenyl)boryl]methane

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Chemical Property of 1,1-bis[dimethylamino(phenyl)boryl]methane

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Technology Process of 1,1-bis[dimethylamino(phenyl)boryl]methane

There total 1 articles about 1,1-bis[dimethylamino(phenyl)boryl]methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1196-44-7
chloro(dimethylamino)phenylborane

: 74-95-3
1,1-dibromomethane

: 1356370-15-4
1,1-bis[dimethylamino(phenyl)boryl]methane

Guidance literature:: With Mg amalgam; In diethyl ether; benzene; under Ar, Schlenk technique; to Mg/Hg added mixt. of Et2O, benzene and CH2Br2, stirred for 20 min; then suspn. mixed with borane, stirred for 5 h at room temp.; more CH2Br added, stirred for 20 h; procedure repeated once more; decanted from alloy; solvent removed in vac.; residue treated with n-pentane; filtered, filtrate dried; distilled at 1 mbar;
DOI:10.1002/zaac.201100322

Reference yield: 82.0%

: 1356370-15-4
1,1-bis[dimethylamino(phenyl)boryl]methane

: 142294-91-5
1,1-bis[(chloro(phenyl)boryl)]methane

Guidance literature:: With hydrogenchloride; In diethyl ether; at 0 ℃; Inert atmosphere;
DOI:10.1002/zaac.201100322

Reference yield: 82.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 1356370-15-4
1,1-bis[dimethylamino(phenyl)boryl]methane

: 142294-91-5
1,1-bis[(chloro(phenyl)boryl)]methane

Guidance literature:: In diethyl ether; under Ar; Schlenk techniaue; boron compd. dissolved in Et2O, treated with dry HCl gas; stirred overnight; filtered, volatile components removed from filtrate in vac.; residue treated with pentane; filtered, dried, distilled at 0.1 mbar;
DOI:10.1002/zaac.201100322