N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) nickel(II)(methyl)(diethyl ether) tetra(3,5-trifluoromethyl phenyl)borate

Base Information

• Chemical Name: N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) nickel(II)(methyl)(diethyl ether) tetra(3,5-trifluoromethyl phenyl)borate
• CAS No.: 252264-25-8
• Molecular Formula: C₃₂H₁₂BF₂₄*C₃₃H₃₇N₂NiO
• Molecular Weight: 1399.58

Synonyms:N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) nickel(II)(methyl)(diethyl ether) tetra(3,5-trifluoromethyl phenyl)borate

Chemical Property of N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) nickel(II)(methyl)(diethyl ether) tetra(3,5-trifluoromethyl phenyl)borate

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Technology Process of N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) nickel(II)(methyl)(diethyl ether) tetra(3,5-trifluoromethyl phenyl)borate

There total 1 articles about N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) nickel(II)(methyl)(diethyl ether) tetra(3,5-trifluoromethyl phenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyloxonium tetrakis[tri(fluoromethyl)phenyl]borate (1134299-66-3) + [C28H24N2Ni(CH3)2] (252264-23-6) → N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) nickel(II)(methyl)(diethyl ether) tetra(3,5-trifluoromethyl phenyl)borate (252264-25-8)

Guidance literature:

In diethyl ether; -130°C;

DOI:10.1021/ja991931h

Reference yield: 100.0%

N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) nickel(II)(methyl)(diethyl ether) tetra(3,5-trifluoromethyl phenyl)borate (252264-25-8) → [C28H24N2Ni(CH3)(H2O)](1+)*[B(C6H3(CF3)2)4](1-)=[C28H24N2Ni(CH3)(H2O)][B(C6H3(CF3)2)4] (252264-29-2)

Guidance literature:

With water; In dichloromethane; -78°C;

DOI:10.1021/ja991931h

Reference yield: 100.0%

ethene (74-85-1) + N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) nickel(II)(methyl)(diethyl ether) tetra(3,5-trifluoromethyl phenyl)borate (252264-25-8) → (C10H6C2(NC6H3(CH3)2)2)Ni(CH3)C2H4(1+) (252264-32-7)

Guidance literature:

In further solvent(s); -110°C, CDCl2F, 3 h, 20 equiv. of C2H4; Kinetics;

DOI:10.1021/ja991931h

upstream raw materials:

diethyloxonium tetrakis[tri(fluoromethyl)phenyl]borate

[C₂₈H₂₄N₂Ni(CH₃)2]

Downstream raw materials:

[C₂₈H₂₄N₂Ni(CH₃)(H₂O)]⁽¹⁺⁾*[B(C₆H₃(CF₃)2)4]^(1-)=[C₂₈H₂₄N₂Ni(CH₃)(H₂O)][B(C₆H₃(CF₃)2)4]

(C₁₀H₆C₂(NC₆H₃(CH₃)2)2)Ni(CH₃)C₂H₄⁽¹⁺⁾

(C₁₀H₆C₂(NC₆H₃(CH₃)2)2)Ni(CH₂CH₂CH₃)⁽¹⁺⁾

(C₁₀H₆C₂(NC₆H₃(CH₃)2)2)Ni(CH₂CH₂CH₃)⁽¹⁺⁾

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