(Z)-2,2'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Base Information

Chemical Name:(Z)-2,2'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
CAS No.:355012-41-8
Molecular Formula:C₂₇H₃₃B₂F₃O₄
Molecular Weight:500.174
Hs Code.:

Synonyms:(Z)-2,2'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2,2'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Technology Process of (Z)-2,2'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

There total 1 articles about (Z)-2,2'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 370-99-0
4-trifluoromethyldiphenylethyne

: 73183-34-3
bis(pinacol)diborane

: 355012-41-8
(Z)-2,2'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: With tetrakis(triphenylphosphine)platinum; In toluene; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1002/anie.202008113

Reference yield: 90.0%

: 106-39-8
bromochlorobenzene

: 355012-41-8
(Z)-2,2'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: (Z)-4,4'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(chlorobenzene)

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate; In 1,4-dioxane; water; at 70 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.202008113

Reference yield: 77.0%

: 355012-41-8
(Z)-2,2'-(1-phenyl-2-(4-(trifluoromethyl)phenyl)ethene-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 13029-09-9
2,2'-dibromobiphenyl

: 1091603-71-2
9-phenyl-10-[4-(trifluoromethyl)phenyl]phenanthrene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 60 ℃; for 48h; Inert atmosphere;
DOI:10.1002/anie.200803213