2-[(2'-oxoazetidin-4'-yl)oxy]ethyl 1,1-dimethyl-2-phenylethanesulfonate

Base Information

Chemical Name:2-[(2'-oxoazetidin-4'-yl)oxy]ethyl 1,1-dimethyl-2-phenylethanesulfonate
CAS No.:810668-13-4
Molecular Formula:C₁₅H₂₁NO₅S
Molecular Weight:327.401
Hs Code.:

Synonyms:2-[(2'-oxoazetidin-4'-yl)oxy]ethyl 1,1-dimethyl-2-phenylethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(2'-oxoazetidin-4'-yl)oxy]ethyl 1,1-dimethyl-2-phenylethanesulfonate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-[(2'-oxoazetidin-4'-yl)oxy]ethyl 1,1-dimethyl-2-phenylethanesulfonate

There total 2 articles about 2-[(2'-oxoazetidin-4'-yl)oxy]ethyl 1,1-dimethyl-2-phenylethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1189-71-5
isocyanate de chlorosulfonyle

: 1-vinyloxethyl 1,1-dimethyl-2-phenylethanesulfonate

: 810668-13-4
2-[(2'-oxoazetidin-4'-yl)oxy]ethyl 1,1-dimethyl-2-phenylethanesulfonate

Guidance literature:: With sodium carbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; at -70 ℃; for 0.5h;
DOI:10.1002/ejoc.200400226

Reference yield:

: 810668-09-8
1-vinyloxethyl propane 2-sulfonate

: 810668-13-4
2-[(2'-oxoazetidin-4'-yl)oxy]ethyl 1,1-dimethyl-2-phenylethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / nBuLi; DMPU / hexane; tetrahydrofuran / 3 h / -70 °C

2: 50 percent / Na₂CO₃; Red-Al / toluene / 0.5 h / -70 °C

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; n-butyllithium; sodium carbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; hexane; toluene;
DOI:10.1002/ejoc.200400226