diethylmethylsilyl acetate

Base Information

• Chemical Name: diethylmethylsilyl acetate
• CAS No.: 5290-28-8
• Molecular Formula: C₇H₁₆O₂Si
• Molecular Weight: 160.288
• Mol file: 5290-28-8.mol

Synonyms:diethylmethylsilyl acetate

Chemical Property of diethylmethylsilyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of diethylmethylsilyl acetate

There total 3 articles about diethylmethylsilyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethylmethylsilane (760-32-7) + carbon monoxide (201230-82-2) + cyclohexyl acetate (622-45-7) → diethylmethylsilyl acetate (5290-28-8) + Cyclohexylidenemethoxy-diethyl-methyl-silane (61490-91-3)

Guidance literature:

With dicobalt octacarbonyl; In benzene; at 200 ℃; for 6h;

DOI:10.1021/ja00343a050

Reference yield:

diethylmethylsilane (760-32-7) + carbon monoxide (201230-82-2) + 4-chlorocyclohexanol acetate (84454-61-5) → diethylmethylsilyl acetate (5290-28-8) + <(4-chlorocyclohexylidene)methoxy>diethylmethylsilane (84454-50-2)

Guidance literature:

With dicobalt octacarbonyl; In benzene; at 200 ℃; for 6h;

DOI:10.1021/ja00343a050

Reference yield:

diethylmethylsilane (760-32-7) + carbon monoxide (201230-82-2) + Acetic acid 2-(4-tert-butyl-phenyl)-1-methyl-ethyl ester (84454-49-9) → diethylmethylsilyl acetate (5290-28-8) + diethyl<<3-<4-(1,1-dimethylethyl)phenyl>-2-methyl-1-propenyl>oxy>methylsilane (84472-74-2,84472-75-3)

Guidance literature:

With dicobalt octacarbonyl; In benzene; at 200 ℃; for 6h;

DOI:10.1021/ja00343a050

upstream raw materials:

diethylmethylsilane

carbon monoxide

cyclohexyl acetate

4-chlorocyclohexanol acetate

Downstream raw materials:

Bis(diethylmethylsilyl)-α-chlorobenzylphosphonat