isophthalic acid L-prolyl-2(S)-(acetoxyacetyl)pyrrolidine L-prolyl-pyrrolidine amide

Base Information

Chemical Name:isophthalic acid L-prolyl-2(S)-(acetoxyacetyl)pyrrolidine L-prolyl-pyrrolidine amide
CAS No.:473797-91-0
Molecular Formula:C₃₀H₃₈N₄O₇
Molecular Weight:566.654
Hs Code.:

Synonyms:isophthalic acid L-prolyl-2(S)-(acetoxyacetyl)pyrrolidine L-prolyl-pyrrolidine amide

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Chemical Property of isophthalic acid L-prolyl-2(S)-(acetoxyacetyl)pyrrolidine L-prolyl-pyrrolidine amide

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Technology Process of isophthalic acid L-prolyl-2(S)-(acetoxyacetyl)pyrrolidine L-prolyl-pyrrolidine amide

There total 7 articles about isophthalic acid L-prolyl-2(S)-(acetoxyacetyl)pyrrolidine L-prolyl-pyrrolidine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1877-71-0
benzene 1,3-dicarboxylic acid monomethyl ester

: 473797-91-0
isophthalic acid L-prolyl-2(S)-(acetoxyacetyl)pyrrolidine L-prolyl-pyrrolidine amide

Guidance literature:: Multi-step reaction with 7 steps

1: Et₃N / CH₂Cl₂ / 1 h / 0 °C

2: Et₃N / CH₂Cl₂ / 20 °C

3: aq. LiOH / methanol / 20 °C

4: Et₃N / CH₂Cl₂ / 1 h / 0 °C

5: aq. LiOH / methanol / 20 °C

6: Et₃N / CH₂Cl₂ / 1 h / 0 °C

7: Et₃N / CH₂Cl₂ / 20 h

With lithium hydroxide; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm020966g

Reference yield:

: C₁₄H₁₆O₅

: 473797-91-0
isophthalic acid L-prolyl-2(S)-(acetoxyacetyl)pyrrolidine L-prolyl-pyrrolidine amide

Guidance literature:: Multi-step reaction with 6 steps

1: Et₃N / CH₂Cl₂ / 20 °C

2: aq. LiOH / methanol / 20 °C

3: Et₃N / CH₂Cl₂ / 1 h / 0 °C

4: aq. LiOH / methanol / 20 °C

5: Et₃N / CH₂Cl₂ / 1 h / 0 °C

6: Et₃N / CH₂Cl₂ / 20 h

With lithium hydroxide; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm020966g

Reference yield:

: 473797-79-4
3-[(S)-2-(Pyrrolidine-1-carbonyl)-pyrrolidine-1-carbonyl]-benzoic acid methyl ester

: 473797-91-0
isophthalic acid L-prolyl-2(S)-(acetoxyacetyl)pyrrolidine L-prolyl-pyrrolidine amide

Guidance literature:: Multi-step reaction with 5 steps

1: aq. LiOH / methanol / 20 °C

2: Et₃N / CH₂Cl₂ / 1 h / 0 °C

3: aq. LiOH / methanol / 20 °C

4: Et₃N / CH₂Cl₂ / 1 h / 0 °C

5: Et₃N / CH₂Cl₂ / 20 h

With lithium hydroxide; triethylamine; In methanol; dichloromethane;
DOI:10.1021/jm020966g