4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)(methyl)carbamate

Base Information

Chemical Name:4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)(methyl)carbamate
CAS No.:1315321-58-4
Molecular Formula:C₂₅H₂₄ClNO₄S
Molecular Weight:469.989
Hs Code.:

Synonyms:4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)(methyl)carbamate

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Chemical Property of 4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)(methyl)carbamate

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Technology Process of 4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)(methyl)carbamate

There total 2 articles about 4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)(methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1315321-56-2
4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)carbamate

: 77-78-1
dimethyl sulfate

: 1315321-58-4
4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)(methyl)carbamate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.1039/c0ob01156h

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 40312-34-3
(2-Amino-4,5,6,7-tetrahydrobenzo[b]thiophen-3-yl)(4-chlorophenyl)methanone

: 1315321-58-4
4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)(methyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 2 h

1.2: 3.5 h

2.1: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / Inert atmosphere

With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/c0ob01156h