4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)carbamate

Base Information

Chemical Name:4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)carbamate
CAS No.:1315321-56-2
Molecular Formula:C₂₄H₂₂ClNO₄S
Molecular Weight:455.962
Hs Code.:

Synonyms:4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)carbamate

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Technology Process of 4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)carbamate

There total 1 articles about 4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 124-38-9,18923-20-1
carbon dioxide

: 824-94-2
p-methoxybenzyl chloride

: 40312-34-3
(2-Amino-4,5,6,7-tetrahydrobenzo[b]thiophen-3-yl)(4-chlorophenyl)methanone

: 1315321-56-2
4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)carbamate

: 1315321-57-3
C₃₂H₃₀ClNO₅S

Guidance literature:: carbon dioxide; (2-Amino-4,5,6,7-tetrahydrobenzo[b]thiophen-3-yl)(4-chlorophenyl)methanone; With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; for 2h;

p-methoxybenzyl chloride; In N,N-dimethyl-formamide; for 3.5h;
DOI:10.1039/c0ob01156h

Reference yield: 92.0%

: 1315321-56-2
4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)carbamate

: 77-78-1
dimethyl sulfate

: 1315321-58-4
4-methoxybenzyl (3-(4-chlorobenzoyl)-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)(methyl)carbamate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; Inert atmosphere;
DOI:10.1039/c0ob01156h