C₅₄H₄₂BF₂N₃O₆S₂

Base Information

Chemical Name:C₅₄H₄₂BF₂N₃O₆S₂
CAS No.:1533402-20-8
Molecular Formula:C₅₄H₄₂BF₂N₃O₆S₂
Molecular Weight:941.884
Hs Code.:

C<sub>54</sub>H<sub>42</sub>BF<sub>2</sub>N<sub>3</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₅₄H₄₂BF₂N₃O₆S₂

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Chemical Property of C₅₄H₄₂BF₂N₃O₆S₂

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Technology Process of C₅₄H₄₂BF₂N₃O₆S₂

There total 7 articles about C₅₄H₄₂BF₂N₃O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 109-63-7
boron trifluoride diethyl etherate

: 1533402-16-2
C₂₇H₂₃NO₃S

: 1533402-20-8
C₅₄H₄₂BF₂N₃O₆S₂

Guidance literature:: C₂₇H₂₃NO₃S; With acetic anhydride; acetic acid; sodium nitrite; at 0 - 80 ℃;

boron trifluoride diethyl etherate; With triethylamine; In toluene; at 20 - 80 ℃;
DOI:10.1039/c6nj01011c

Reference yield:

: 109-63-7
boron trifluoride diethyl etherate

: C₅₄H₄₃N₃O₆S₂

: 1533402-20-8
C₅₄H₄₂BF₂N₃O₆S₂

Guidance literature:: With triethylamine; In toluene; at 80 ℃; for 0.5h;
DOI:10.1021/ol4034622

Reference yield:

: 46193-76-4
ethyl 4H-thieno[3,2-b]pyrrole-5-carboxylate

: 1533402-20-8
C₅₄H₄₂BF₂N₃O₆S₂

Guidance literature:: Multi-step reaction with 5 steps

1: bromine / dichloromethane / 1 h

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene / 12 h / Inert atmosphere; Schlenk technique; Heating

3: potassium hydroxide / ethylene glycol / 2 h / 130 °C / Inert atmosphere

4: acetic acid; acetic anhydride; sodium nitrite / 1.25 h / 0 - 80 °C

5: triethylamine / toluene / 0.5 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; acetic anhydride; sodium carbonate; acetic acid; triethylamine; potassium hydroxide; sodium nitrite; In dichloromethane; ethylene glycol; toluene; 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol4034622