Technology Process of 3,4-bis(benzyloxy)-2-methyl-6,β-dinitrostyrene
There total 5 articles about 3,4-bis(benzyloxy)-2-methyl-6,β-dinitrostyrene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
nitric acid;
In
acetic acid;
for 2.5h;
Ambient temperature;
DOI:10.1021/jm00147a027
- Guidance literature:
-
Multi-step reaction with 5 steps
1: TiCl4 / CH2Cl2 / 2 h / 25 °C
2: BBr3 / CH2Cl2 / 1.) -78 deg C, 30 min, 2.) 25 deg C, 2 h
3: 76 percent / KI, K2CO3 / acetone / 7 h / Heating
4: 86 percent / NH4OAc / acetic acid / 1.5 h / Heating
5: 82 percent / 90percent HNO3 / acetic acid / 2.5 h / Ambient temperature
With
ammonium acetate; nitric acid; boron tribromide; titanium tetrachloride; potassium carbonate; potassium iodide;
In
dichloromethane; acetic acid; acetone;
DOI:10.1021/jm00147a027
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 76 percent / KI, K2CO3 / acetone / 7 h / Heating
2: 86 percent / NH4OAc / acetic acid / 1.5 h / Heating
3: 82 percent / 90percent HNO3 / acetic acid / 2.5 h / Ambient temperature
With
ammonium acetate; nitric acid; potassium carbonate; potassium iodide;
In
acetic acid; acetone;
DOI:10.1021/jm00147a027
