2,3-Dimethoxytoluene

Base Information

Chemical Name:2,3-Dimethoxytoluene
CAS No.:4463-33-6
Molecular Formula:C9H12O2
Molecular Weight:152.193
Hs Code.:
European Community (EC) Number:224-726-4
NSC Number:72350
DSSTox Substance ID:DTXSID40196259
Nikkaji Number:J150.000G
Wikidata:Q83069315
Mol file:4463-33-6.mol

Synonyms:dimethoxytoluene

Suppliers and Price of 2,3-Dimethoxytoluene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,3-Dimethoxytoluene
1g
$ 50.00

TRC
2,3-Dimethoxytoluene
25g
$ 305.00

Sigma-Aldrich
2,3-Dimethoxytoluene 99%
25g
$ 277.00

Crysdot
1,2-Dimethoxy-3-methylbenzene 97%
500g
$ 749.00

ChemScene
Toluene,2,3-dimethoxy- 98.15%
25g
$ 98.00

Chemenu
1,2-Dimethoxy-3-methylbenzene 95+%
500g
$ 700.00

Biosynth Carbosynth
2,3-Dimethoxytoluene
250 g
$ 680.00

Biosynth Carbosynth
2,3-Dimethoxytoluene
100 g
$ 300.00

Biosynth Carbosynth
2,3-Dimethoxytoluene
50 g
$ 165.00

Biosynth Carbosynth
2,3-Dimethoxytoluene
25 g
$ 92.50

Total 31 raw suppliers

Chemical Property of 2,3-Dimethoxytoluene

Chemical Property:

Vapor Pressure:0.438mmHg at 25°C
Melting Point:202-203°C
Refractive Index:n20/D 1.514(lit.)
Boiling Point:201.4 °C at 760 mmHg
Flash Point:67.6 °C
PSA：18.46000
Density:0.99g/cm³
LogP:2.01220
Storage Temp.:Sealed in dry,Room Temperature
Water Solubility.:Soluble in Dichloromethane. Not miscible in water.
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:152.083729621
Heavy Atom Count:11
Complexity:114

Purity/Quality:

97% ^*data from raw suppliers

2,3-Dimethoxytoluene ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)OC)OC
Uses 2,3-Dimethoxytoluene has been used to prepare 6,7-dimethoxy-4-hydroxyisochroman-3-one.

Technology Process of 2,3-Dimethoxytoluene

There total 17 articles about 2,3-Dimethoxytoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 91-16-7
1,2-dimethoxybenzene

: 74-88-4
methyl iodide

: 4463-33-6
1,2-dimethoxy-3-methylbenzene

Guidance literature:: 1,2-dimethoxybenzene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; Inert atmosphere;
DOI:10.1002/chem.202101863

Reference yield: 98.0%

: 86-51-1
2,3-dimethyoxybenzaldehyde

: 4463-33-6
1,2-dimethoxy-3-methylbenzene

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 0.75h; under 760.051 Torr;
DOI:10.1016/j.tet.2007.06.105

Reference yield: 96.0%

: 5653-67-8
2,3-dimethoxybenzyl alcohol

: 4463-33-6
1,2-dimethoxy-3-methylbenzene

Guidance literature:: 2,3-dimethoxybenzyl alcohol; With ammonium formate; In ethanol; water; at 22 ℃; for 0.166667h;

With formic acid; In ethanol; water; at 22 ℃; for 4h; chemoselective reaction;
DOI:10.1055/s-0040-1707398