Technology Process of 2,3-Dimethoxytoluene
There total 17 articles about 2,3-Dimethoxytoluene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,2-dimethoxybenzene;
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
methyl iodide;
In
tetrahydrofuran;
Inert atmosphere;
DOI:10.1002/chem.202101863
- Guidance literature:
-
With
hydrogenchloride; hydrogen;
palladium on activated charcoal;
In
methanol;
at 20 ℃;
for 0.75h;
under 760.051 Torr;
DOI:10.1016/j.tet.2007.06.105
- Guidance literature:
-
2,3-dimethoxybenzyl alcohol;
With
ammonium formate;
In
ethanol; water;
at 22 ℃;
for 0.166667h;
With
formic acid;
In
ethanol; water;
at 22 ℃;
for 4h;
chemoselective reaction;
DOI:10.1055/s-0040-1707398
Xi
