N-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine

Base Information

Chemical Name:N-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine
CAS No.:188402-34-8
Molecular Formula:C₁₇H₂₁NO₅
Molecular Weight:319.357
Hs Code.:

Synonyms:N-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine

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Technology Process of N-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine

There total 3 articles about N-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 188402-33-7
N-benzyl-3-O-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine

: 188402-34-8
N-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 5h;
DOI:10.1080/07328309708006510

Reference yield:

: 100-39-0
benzyl bromide

: 188402-34-8
N-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / K₂CO₃; tetrabutylammonium bromide / benzene / 1 h / Heating

2: 92 percent / hydrogen / Pd/C / methanol / 5 h

With tetrabutylammomium bromide; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; benzene; 1: Alkylation / 2: Hydrogenolysis;
DOI:10.1080/07328309708006510

Reference yield:

: (1S,3S,4R,5R)-4-Benzyloxy-3-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2-oxa-7-aza-bicyclo[3.2.0]heptan-6-one

: 188402-34-8
N-benzyl-2-C:1-N-carbonyl-2-deoxy-5,6-O-isopropylidene-α-D-glucofuranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / K₂CO₃; tetrabutylammonium bromide / benzene / 1 h / Heating

2: 92 percent / hydrogen / Pd/C / methanol / 5 h

With tetrabutylammomium bromide; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; benzene; 1: Alkylation / 2: Hydrogenolysis;
DOI:10.1080/07328309708006510