2,3-dimethylbutyl phenyl sulfone

Base Information

• Chemical Name: 2,3-dimethylbutyl phenyl sulfone
• CAS No.: 134511-53-8
• Molecular Formula: C₁₂H₁₈O₂S
• Molecular Weight: 226.34
• Mol file: 134511-53-8.mol

Synonyms:2,3-dimethylbutyl phenyl sulfone

Chemical Property of 2,3-dimethylbutyl phenyl sulfone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2,3-dimethylbutyl phenyl sulfone

There total 6 articles about 2,3-dimethylbutyl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(2,3-dimethylbutyl)(phenyl)sulfane (91638-67-4) → 2,3-dimethylbutyl phenyl sulfone (134511-53-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 2h; Ambient temperature;

Reference yield:

2,3-dimethylbutanol (19550-30-2,20281-85-0) → 2,3-dimethylbutyl phenyl sulfone (134511-53-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 98 percent / pyridine / 2 h / Ambient temperature

2: 48 percent / CH₃ONa / methanol / Ambient temperature

3: 96 percent / m-chloroperbenzoic acid / CHCl₃ / 2 h / Ambient temperature

With pyridine; sodium methylate; 3-chloro-benzenecarboperoxoic acid; In methanol; chloroform;

Reference yield:

3-methylbutyric acid (503-74-2) → 2,3-dimethylbutyl phenyl sulfone (134511-53-8)

Guidance literature:

Multi-step reaction with 5 steps

1: 1.) butyllithium, disopropylamine, hexamethylphosphorotriamide / 1.) hexane, THF, -5 deg C, 30 min, 2.) hexane, THF, RT, 2 h

2: 75 percent / LiAlH₄ / diethyl ether / -45 - 20 °C

3: 98 percent / pyridine / 2 h / Ambient temperature

4: 48 percent / CH₃ONa / methanol / Ambient temperature

5: 96 percent / m-chloroperbenzoic acid / CHCl₃ / 2 h / Ambient temperature

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; sodium methylate; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; chloroform;

upstream raw materials:

(2,3-dimethylbutyl)(phenyl)sulfane

3-methylbutyric acid

2,3-dimethylbutanol

2,3-dimethylbutyric acid

Downstream raw materials:

C₃₈H₅₆O₆S