1L-(1,3/2,4,6)-6-ethoxycarbonylamido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol

Base Information

Chemical Name:1L-(1,3/2,4,6)-6-ethoxycarbonylamido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol
CAS No.:137555-96-5
Molecular Formula:C₁₂H₂₀N₂O₇
Molecular Weight:304.3
Hs Code.:

Synonyms:1L-(1,3/2,4,6)-6-ethoxycarbonylamido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol

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Chemical Property of 1L-(1,3/2,4,6)-6-ethoxycarbonylamido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol

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Technology Process of 1L-(1,3/2,4,6)-6-ethoxycarbonylamido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol

There total 1 articles about 1L-(1,3/2,4,6)-6-ethoxycarbonylamido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 541-41-3
chloroformic acid ethyl ester

: 137555-75-0
(3aR,4S,5R,7S,7aR)-7-Amino-2,2-dimethyl-5-nitro-hexahydro-benzo[1,3]dioxol-4-ol

: 29881-47-8,68926-59-0,89920-19-4,89920-20-7
1L-(1,3/2,4,6)-4,6-di-(ethoxycarbonylamido)-1,2-O-isopropylidene-1,2,3-cyclohexanetriol

: 137555-94-3
1D-(1,3/2,4,6)-4-ethoxycarbonylamido-6-nitro-1,2,3-cyclohexanetriol

: 137555-96-5
1L-(1,3/2,4,6)-6-ethoxycarbonylamido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol

Guidance literature:: With sodium hydrogencarbonate; In water; at 0 ℃;
DOI:10.1139/v91-231

Reference yield:

: 137555-96-5
1L-(1,3/2,4,6)-6-ethoxycarbonylamido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol

: 137555-91-0
((1S,2R,3R,4S,5R)-2,3,4-Trihydroxy-5-methylamino-cyclohexyl)-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: AcOH, H₂ / PtO₂ / ethanol / 30 h / 760 Torr / Ambient temperature

2: 2 h / Ambient temperature

3: BH₃ / tetrahydrofuran / 5 h / Heating

With borane; hydrogen; acetic acid; platinum(IV) oxide; In tetrahydrofuran; ethanol;
DOI:10.1139/v91-231

Reference yield:

: 137555-96-5
1L-(1,3/2,4,6)-6-ethoxycarbonylamido-1,2-O-isopropylidene-4-nitro-1,2,3-cyclohexanetriol

: 137555-92-1
[(1S,2R,3S,4S,5R)-5-(Acetyl-methyl-amino)-2,3,4-trihydroxy-cyclohexyl]-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: AcOH, H₂ / PtO₂ / ethanol / 30 h / 760 Torr / Ambient temperature

2: 2 h / Ambient temperature

3: 35 percent / BH₃ / tetrahydrofuran / 5 h / Heating

4: Ambient temperature

With borane; hydrogen; acetic acid; platinum(IV) oxide; In tetrahydrofuran; ethanol;
DOI:10.1139/v91-231