N-[[3-benzoyl-4-(2-p-tolylacetylamino)phenylcarbamoyl]methyl]-N-methylcarbamic acid tert-butyl ester

Base Information

Chemical Name:N-[[3-benzoyl-4-(2-p-tolylacetylamino)phenylcarbamoyl]methyl]-N-methylcarbamic acid tert-butyl ester
CAS No.:649748-54-9
Molecular Formula:C₃₀H₃₃N₃O₅
Molecular Weight:515.609
Hs Code.:

Synonyms:N-[[3-benzoyl-4-(2-p-tolylacetylamino)phenylcarbamoyl]methyl]-N-methylcarbamic acid tert-butyl ester

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Chemical Property of N-[[3-benzoyl-4-(2-p-tolylacetylamino)phenylcarbamoyl]methyl]-N-methylcarbamic acid tert-butyl ester

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Technology Process of N-[[3-benzoyl-4-(2-p-tolylacetylamino)phenylcarbamoyl]methyl]-N-methylcarbamic acid tert-butyl ester

There total 1 articles about N-[[3-benzoyl-4-(2-p-tolylacetylamino)phenylcarbamoyl]methyl]-N-methylcarbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 13734-36-6
N-(tert-butoxycarbonyl)sarcosine

: 265648-28-0
N-(4-amino-2-benzoylphenyl)-2-(4-methylphenyl)acetic acid amide

: 649748-54-9
N-[[3-benzoyl-4-(2-p-tolylacetylamino)phenylcarbamoyl]methyl]-N-methylcarbamic acid tert-butyl ester

Guidance literature:: N-(tert-butoxycarbonyl)sarcosine; With 4-methyl-morpholine; isobutyl chloroformate; In N,N-dimethyl-formamide; at -15 ℃; for 0.0833333h;

N-(4-amino-2-benzoylphenyl)-2-(4-methylphenyl)acetic acid amide; In N,N-dimethyl-formamide; at -15 - 20 ℃;
DOI:10.1002/ardp.200300758

Reference yield:

: 649748-54-9
N-[[3-benzoyl-4-(2-p-tolylacetylamino)phenylcarbamoyl]methyl]-N-methylcarbamic acid tert-butyl ester

: N-[2-benzoyl-4-(2-methylamino-acetylamino)-phenyl]-2-p-tolyl-acetamide; hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h;
DOI:10.1002/ardp.200300758

Reference yield:

: 649748-54-9
N-[[3-benzoyl-4-(2-p-tolylacetylamino)phenylcarbamoyl]methyl]-N-methylcarbamic acid tert-butyl ester

: N-{[3-benzoyl-4-(2-p-tolyl-acetylamino)-phenylcarbamoyl]-methyl}-3-biphenyl-4-yl-N-methyl-acrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / dioxane / 1 h / 20 °C

2: 457 mg / toluene / 2 h / Heating

With hydrogenchloride; In 1,4-dioxane; toluene;
DOI:10.1002/ardp.200300758