trans-hydridophenoxobis(tribenzylphosphine)nickel(II)*phenol

Base Information

Chemical Name:trans-hydridophenoxobis(tribenzylphosphine)nickel(II)*phenol
CAS No.:135396-05-3
Molecular Formula:C₆H₆O*C₄₈H₄₈NiOP₂
Molecular Weight:855.659
Hs Code.:

Synonyms:trans-hydridophenoxobis(tribenzylphosphine)nickel(II)*phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-hydridophenoxobis(tribenzylphosphine)nickel(II)*phenol

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Technology Process of trans-hydridophenoxobis(tribenzylphosphine)nickel(II)*phenol

There total 2 articles about trans-hydridophenoxobis(tribenzylphosphine)nickel(II)*phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 135395-96-9
trans-chlorohydridobis(tribenzylphosphine)nickel(II)

: 139-02-6
sodium phenoxide

: 135396-05-3
trans-hydridophenoxobis(tribenzylphosphine)nickel(II)*phenol

Guidance literature:: In tetrahydrofuran; benzene; (N2 atmosphere, Schlenk technique); Ni-compd. is dissolved in THF and benzene, addn. of an excess of NaOPh at 0°C, soln. is stirred for 30 min; solvent is removed under vac., residue is washed with Et2O and extd. with toluene, toluene soln. is layered with pentane and cooled to -20°C in a beaker of MeOH, elem. anal.;