Technology Process of C30H42O5
There total 8 articles about C30H42O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 130 ℃;
for 1h;
Microwave irradiation;
Inert atmosphere;
DOI:10.1021/ol200966z
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 25 - 60 °C / Inert atmosphere
1.2: 15 h / 25 °C / Inert atmosphere
2.1: borane-THF / tetrahydrofuran / 72 h / 0 °C / Inert atmosphere
2.2: 0 - 25 °C / Inert atmosphere
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Microwave irradiation; Inert atmosphere
With
borane-THF; tetrabutyl ammonium fluoride; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
2.1: Hydroboration reaction;
DOI:10.1021/ol200966z
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide / 25 - 60 °C / Inert atmosphere
2.2: 15 h / 25 °C / Inert atmosphere
3.1: borane-THF / tetrahydrofuran / 72 h / 0 °C / Inert atmosphere
3.2: 0 - 25 °C / Inert atmosphere
4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Microwave irradiation; Inert atmosphere
With
sodium tetrahydroborate; borane-THF; tetrabutyl ammonium fluoride; sodium hydride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
3.1: Hydroboration reaction;
DOI:10.1021/ol200966z