4-(4-diethylamino-2,6-dimethylphenylimino)-1,4-dihydronaphthylidenemalononitrile

Base Information

Chemical Name:4-(4-diethylamino-2,6-dimethylphenylimino)-1,4-dihydronaphthylidenemalononitrile
CAS No.:129371-69-3
Molecular Formula:C₂₅H₂₄N₄
Molecular Weight:380.492
Hs Code.:

Synonyms:4-(4-diethylamino-2,6-dimethylphenylimino)-1,4-dihydronaphthylidenemalononitrile

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Chemical Property of 4-(4-diethylamino-2,6-dimethylphenylimino)-1,4-dihydronaphthylidenemalononitrile

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Technology Process of 4-(4-diethylamino-2,6-dimethylphenylimino)-1,4-dihydronaphthylidenemalononitrile

There total 4 articles about 4-(4-diethylamino-2,6-dimethylphenylimino)-1,4-dihydronaphthylidenemalononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 5518-09-2
2-(naphthalen-1-yl)malononitrile

: 2359-40-2
2,6-dimethyl-4-(diethylamino)aniline

: 129371-69-3
4-(4-diethylamino-2,6-dimethylphenylimino)-1,4-dihydronaphthylidenemalononitrile

Guidance literature:: With ammonium peroxydisulfate; In ammonium hydroxide; acetone; for 0.5h; Ambient temperature;
DOI:10.1021/ja00008a012

Reference yield:

: 3995-39-9
N,N-diethyl-3,5-dimethylaniline

: 129371-69-3
4-(4-diethylamino-2,6-dimethylphenylimino)-1,4-dihydronaphthylidenemalononitrile

Guidance literature:: Multi-step reaction with 3 steps

1: NaNO₂, conc. HCl / H₂O / 1 h / 0 °C

2: Zn, aq. conc. HCl / 1 h

3: 25 percent / aq. (NH₄)2S₂O₈ / acetone; aq. NH₃ / 0.5 h / Ambient temperature

With hydrogenchloride; ammonium peroxydisulfate; zinc; sodium nitrite; In ammonium hydroxide; water; acetone;
DOI:10.1021/ja00008a012

Reference yield:

: 723733-82-2
(3,5-Dimethyl-4-nitro-phenyl)-diethyl-amine

: 129371-69-3
4-(4-diethylamino-2,6-dimethylphenylimino)-1,4-dihydronaphthylidenemalononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: Zn, aq. conc. HCl / 1 h

2: 25 percent / aq. (NH₄)2S₂O₈ / acetone; aq. NH₃ / 0.5 h / Ambient temperature

With hydrogenchloride; ammonium peroxydisulfate; zinc; In ammonium hydroxide; acetone;
DOI:10.1021/ja00008a012