(E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde

Base Information

Chemical Name:(E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde
CAS No.:1312366-31-6
Molecular Formula:C₁₀H₁₀O₂
Molecular Weight:162.188
Hs Code.:

Synonyms:(E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde

Suppliers and Price of (E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of (E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde

There total 3 articles about (E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 20655-58-7,92636-30-1,62174-99-6
ethyl (E)-4-cyanocinnamate

: 1312366-31-6
(E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde

Guidance literature:: With diisobutylaluminium hydride; In hexane; toluene; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201101078

Reference yield:

: 623-00-7
4-bromobenzenecarbonitrile

: 1312366-31-6
(E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); tetrabutylammomium bromide; sodium acetate / N,N-dimethyl-formamide / 12 h / 140 °C / Inert atmosphere

2: diisobutylaluminium hydride / hexane; toluene / 2 h / 0 °C / Inert atmosphere

With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); tetrabutylammomium bromide; sodium acetate; diisobutylaluminium hydride; In hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201101078

Reference yield:

: 623-27-8
terephthalaldehyde,

: 1312366-31-6
(E)-4-(3-hydroxyprop-1-en-1-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 0.75 h / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; toluene;
DOI:10.1021/ja4083182