3-Benzyl-7-oxy-3H-purin-6-ylamine

Base Information

• Chemical Name: 3-Benzyl-7-oxy-3H-purin-6-ylamine
• CAS No.: 155854-86-7
• Molecular Formula: C₁₂H₁₁N₅O
• Molecular Weight: 241.252
• Mol file: 155854-86-7.mol

Synonyms:3-Benzyl-7-oxy-3H-purin-6-ylamine

Chemical Property of 3-Benzyl-7-oxy-3H-purin-6-ylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Benzyl-7-oxy-3H-purin-6-ylamine

There total 3 articles about 3-Benzyl-7-oxy-3H-purin-6-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

3-benzyladenine (7280-81-1) → 3-Benzyl-7-oxy-3H-purin-6-ylamine (155854-86-7)

Guidance literature:

With magnesium monoperoxyphthalate hexahydrate; In methanol; at 30 ℃; for 20h;

DOI:10.1248/cpb.43.53

Reference yield:

adenine (66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9) → 3-Benzyl-7-oxy-3H-purin-6-ylamine (155854-86-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 53 percent / AcNMe₂ / pH >7

2: 40 percent / magnesium monoperoxyphthalate hexahydrate / methanol / 20 h / 30 °C

With N,N-dimethyl acetamide; magnesium monoperoxyphthalate hexahydrate; In methanol;

Reference yield:

3-benzyladenine (7280-81-1) + acetonitrile (75-05-8,26809-02-9) → 3-Benzyl-7-oxy-3H-purin-6-ylamine (155854-86-7) + 7-acetamido-3-benzyladenine

Guidance literature:

With dihydrogen peroxide; potassium hydrogencarbonate; Yield given. Multistep reaction. Yields of byproduct given; 1.) MeOH, 25 deg C, 22 h, 2.) H₂O, catalase (from bovine liver), 25 deg C, 6 h;

DOI:10.1248/cpb.43.53

upstream raw materials:

3-benzyladenine

acetonitrile

adenine

Downstream raw materials:

3-methyladenine

diceto-6,8 purine

6-Amino-3-benzyl-3H-purin-8-ol

adenine 7-oxide