1-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,2,2-tris-methylsulfanyl-ethanone

Base Information

Chemical Name:1-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,2,2-tris-methylsulfanyl-ethanone
CAS No.:171897-81-7
Molecular Formula:C₁₅H₁₇NO₃S₄
Molecular Weight:387.569
Hs Code.:

Synonyms:1-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,2,2-tris-methylsulfanyl-ethanone

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Chemical Property of 1-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,2,2-tris-methylsulfanyl-ethanone

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Technology Process of 1-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,2,2-tris-methylsulfanyl-ethanone

There total 3 articles about 1-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,2,2-tris-methylsulfanyl-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40167-20-2
N-(methylthio)phthalimide

: 5418-86-0
tris(methylthio)methane

: 57850-02-9
methyl 1-(phenylsulfonyl)-1H-pyrrole-2-carboxylate

: 171897-81-7
1-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,2,2-tris-methylsulfanyl-ethanone

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, -95 deg C, 2 h; -45 deg C, 30 min, 2.) r.t., 1 h;
DOI:10.1021/jo00124a009

Reference yield:

: 1193-62-0
methyl Pyrrole-2-carboxylate

: 171897-81-7
1-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,2,2-tris-methylsulfanyl-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / tetrabutylammonium hydrogen sulfate, 50percent aq. NaOH / CH₂Cl₂ / 0.5 h

2: 1.) BuLi / 1.) THF, hexane, -95 deg C, 2 h; -45 deg C, 30 min, 2.) r.t., 1 h

With sodium hydroxide; n-butyllithium; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane;
DOI:10.1021/jo00124a009

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 171897-81-7
1-(1-Benzenesulfonyl-1H-pyrrol-2-yl)-2,2,2-tris-methylsulfanyl-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / tetrabutylammonium hydrogen sulfate, 50percent aq. NaOH / CH₂Cl₂ / 0.5 h

2: 1.) BuLi / 1.) THF, hexane, -95 deg C, 2 h; -45 deg C, 30 min, 2.) r.t., 1 h

With sodium hydroxide; n-butyllithium; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane;
DOI:10.1021/jo00124a009