but-3-en-1-yl 4-bromobenzoate

Base Information

• Chemical Name: but-3-en-1-yl 4-bromobenzoate
• CAS No.: 1333159-60-6
• Molecular Formula: C₁₁H₁₁BrO₂
• Molecular Weight: 255.111
• Mol file: 1333159-60-6.mol

Synonyms:but-3-en-1-yl 4-bromobenzoate

Chemical Property of but-3-en-1-yl 4-bromobenzoate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of but-3-en-1-yl 4-bromobenzoate

There total 2 articles about but-3-en-1-yl 4-bromobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

homoalylic alcohol (627-27-0) + 4-Bromobenzoic acid (586-76-5) → but-3-en-1-yl 4-bromobenzoate (1333159-60-6)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 22 ℃; for 12h;

DOI:10.1055/s-0036-1591944

Reference yield:

homoalylic alcohol (627-27-0) + 4-chlorobenzoyl chloride (586-75-4) → but-3-en-1-yl 4-bromobenzoate (1333159-60-6)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ja206330m

Reference yield: 85.0%

cyclohexane (110-82-7,25012-93-5) + but-3-en-1-yl 4-bromobenzoate (1333159-60-6) → 4-cyclohexylbutyl 4-bromobenzoate

Guidance literature:

With copper (II)-fluoride; for 16h; Reflux; Sealed tube;

DOI:10.1039/c8gc01394b

upstream raw materials:

homoalylic alcohol

4-chlorobenzoyl chloride

4-Bromobenzoic acid

Downstream raw materials:

(E)-5,5,5-trifluoropent-2-enyl 4-bromobenzoate