2-Cyclohexen-1-ol,1-methyl-4-[(1R)-1,2,2-trimethylcyclopentyl]-,(1R,4R)-rel-(9CI)

Base Information

Chemical Name:2-Cyclohexen-1-ol,1-methyl-4-[(1R)-1,2,2-trimethylcyclopentyl]-,(1R,4R)-rel-(9CI)
CAS No.:807375-34-4
Molecular Formula:C₁₅H₂₆O
Molecular Weight:222.371
Hs Code.:
Mol file:807375-34-4.mol

Synonyms:2-Cyclohexen-1-ol,1-methyl-4-[(1R)-1,2,2-trimethylcyclopentyl]-,(1R,4R)-rel-(9CI)

Suppliers and Price of 2-Cyclohexen-1-ol,1-methyl-4-[(1R)-1,2,2-trimethylcyclopentyl]-,(1R,4R)-rel-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyclohexen-1-ol,1-methyl-4-[(1R)-1,2,2-trimethylcyclopentyl]-,(1R,4R)-rel-(9CI)

Chemical Property:

PSA：20.23000
LogP:3.92000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Cyclohexen-1-ol,1-methyl-4-[(1R)-1,2,2-trimethylcyclopentyl]-,(1R,4R)-rel-(9CI)

There total 73 articles about 2-Cyclohexen-1-ol,1-methyl-4-[(1R)-1,2,2-trimethylcyclopentyl]-,(1R,4R)-rel-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 807377-62-4
4-(4-methoxyphenyl)-4,5,5-trimethylcyclopent-2-enone

: 807375-34-4,807375-46-8,807375-56-0,807375-67-3
(+/-)-cuprenenol

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen / Pd/C / ethanol / 3 h / 20 °C

2.1: 95 mg / BF₃*OEt₂ / benzene / 12 h / 0 - 20 °C

3.1: Raney nickel / ethanol / 2 h / Heating

4.1: lithium; liq. ammonia / ethanol; tetrahydrofuran / 2.5 h

5.1: 147 mg / sulphuric acid / tetrahydrofuran; H₂O / 0.83 h / 20 °C

6.1: 90 percent / rhodium chloride trihydrate / ethanol / 3 h / 100 - 110 °C

7.1: magnesium; iodine / diethyl ether

7.2: diethyl ether / 0 - 20 °C

With rhodium(III) chloride; sulfuric acid; boron trifluoride diethyl etherate; ammonia; hydrogen; iodine; lithium; nickel; magnesium; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; water; benzene; 4.1: Birch reduction;
DOI:10.1081/SCC-200034755

Reference yield:

: 807377-62-4
4-(4-methoxyphenyl)-4,5,5-trimethylcyclopent-2-enone

: 807375-34-4,807375-46-8,807375-56-0,807375-67-3
neocuprenenol

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen / Pd/C / ethanol / 3 h / 20 °C

2.1: 95 mg / BF₃*OEt₂ / benzene / 12 h / 0 - 20 °C

3.1: Raney nickel / ethanol / 2 h / Heating

4.1: lithium; liq. ammonia / ethanol; tetrahydrofuran / 2.5 h

5.1: 147 mg / sulphuric acid / tetrahydrofuran; H₂O / 0.83 h / 20 °C

6.1: 90 percent / rhodium chloride trihydrate / ethanol / 3 h / 100 - 110 °C

7.1: magnesium; iodine / diethyl ether

7.2: diethyl ether / 0 - 20 °C

With rhodium(III) chloride; sulfuric acid; boron trifluoride diethyl etherate; ammonia; hydrogen; iodine; lithium; nickel; magnesium; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; water; benzene; 4.1: Birch reduction;
DOI:10.1081/SCC-200034755

Reference yield:

: 807377-62-4
4-(4-methoxyphenyl)-4,5,5-trimethylcyclopent-2-enone

: 807375-34-4,807375-46-8,807375-56-0,807375-67-3
(+/-)-infuscol B

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen / Pd/C / ethanol / 3 h / 20 °C

2.1: 95 mg / BF₃*OEt₂ / benzene / 12 h / 0 - 20 °C

3.1: Raney nickel / ethanol / 2 h / Heating

4.1: lithium; liq. ammonia / ethanol; tetrahydrofuran / 2.5 h

5.1: 147 mg / sulphuric acid / tetrahydrofuran; H₂O / 0.83 h / 20 °C

6.1: 90 percent / rhodium chloride trihydrate / ethanol / 3 h / 100 - 110 °C

7.1: magnesium; iodine / diethyl ether

7.2: diethyl ether / 0 - 20 °C

With rhodium(III) chloride; sulfuric acid; boron trifluoride diethyl etherate; ammonia; hydrogen; iodine; lithium; nickel; magnesium; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; water; benzene; 4.1: Birch reduction;
DOI:10.1081/SCC-200034755