C₂₉H₂₉NO

Base Information

Chemical Name:C₂₉H₂₉NO
CAS No.:305822-73-5
Molecular Formula:C₂₉H₂₉NO
Molecular Weight:407.555
Hs Code.:

Synonyms:C₂₉H₂₉NO

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Chemical Property of C₂₉H₂₉NO

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Technology Process of C₂₉H₂₉NO

There total 9 articles about C₂₉H₂₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: trifluoromethanesulfonic acid [4bS-(4bα,7α,8aβ)]-4b,5,6,7,8,8a,9,10-octahydro-7-hydroxy-4b-(phenylmethyl)-7-(1-propynyl)-2-phenanthrenyl ester

: pyridin-2-ylzinc(II) bromide

: 305822-73-5
C₂₉H₂₉NO

Guidance literature:: trifluoromethanesulfonic acid [4bS-(4bα,7α,8aβ)]-4b,5,6,7,8,8a,9,10-octahydro-7-hydroxy-4b-(phenylmethyl)-7-(1-propynyl)-2-phenanthrenyl ester; With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; In tetrahydrofuran; for 0.0833333h; Inert atmosphere;

pyridin-2-ylzinc(II) bromide; In tetrahydrofuran; at -78 - 70 ℃;

Reference yield:

: 1-benzyl-6-methoxy-1-(3-oxo-butyl)-3,4-dihydro-1H-naphthalen-2-one

: 305822-73-5
C₂₉H₂₉NO

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium methylate / methanol / 3.25 h / 20 - 75 °C

2.1: tetra-(n-butyl)ammonium iodide; boron trichloride / dichloromethane / 1.5 h / -78 - 20 °C / Inert atmosphere

3.1: ammonia; lithium / 1,4-dioxane; diethyl ether / 0.5 h / -78 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

4.2: 20 °C

5.1: 2,6-dimethylpyridine; dmap / dichloromethane / 2.5 h / -40 - 20 °C / Inert atmosphere

6.1: palladium diacetate; 1,1'-bis-(diphenylphosphino)ferrocene / tetrahydrofuran / 0.08 h / Inert atmosphere

6.2: -78 - 70 °C

With 2,6-dimethylpyridine; dmap; 1,1'-bis-(diphenylphosphino)ferrocene; ammonia; sodium methylate; palladium diacetate; boron trichloride; tetra-(n-butyl)ammonium iodide; lithium; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane;

Reference yield:

: 305822-65-5
CP-409069

: 305822-73-5
C₂₉H₂₉NO

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,6-dimethylpyridine; dmap / dichloromethane / 2.5 h / -40 - 20 °C / Inert atmosphere

2.1: palladium diacetate; 1,1'-bis-(diphenylphosphino)ferrocene / tetrahydrofuran / 0.08 h / Inert atmosphere

2.2: -78 - 70 °C

With 2,6-dimethylpyridine; dmap; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; In tetrahydrofuran; dichloromethane;