ethyl (2S,3R)-3-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate

Base Information

Chemical Name:ethyl (2S,3R)-3-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate
CAS No.:1350705-68-8
Molecular Formula:C₂₃H₂₉NO₆
Molecular Weight:415.486
Hs Code.:

Synonyms:ethyl (2S,3R)-3-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate

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Chemical Property of ethyl (2S,3R)-3-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate

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Technology Process of ethyl (2S,3R)-3-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate

There total 3 articles about ethyl (2S,3R)-3-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4397-53-9
p-benzyloxybenzaldehyde

: 1350705-68-8
ethyl (2S,3R)-3-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: water / 2 h / 90 °C / Inert atmosphere

2.1: tert-butylhypochlorite; sodium hydroxide / propan-1-ol; water / 0.08 h / Inert atmosphere

2.2: 2 h / Inert atmosphere

With tert-butylhypochlorite; sodium hydroxide; In propan-1-ol; water;
DOI:10.1039/c1ob06320k

Reference yield:

: 100-39-0
benzyl bromide

: 1350705-68-8
ethyl (2S,3R)-3-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / Inert atmosphere

2.1: water / 2 h / 90 °C / Inert atmosphere

3.1: tert-butylhypochlorite; sodium hydroxide / propan-1-ol; water / 0.08 h / Inert atmosphere

3.2: 2 h / Inert atmosphere

With tert-butylhypochlorite; tetra-(n-butyl)ammonium iodide; potassium carbonate; sodium hydroxide; In propan-1-ol; water;
DOI:10.1039/c1ob06320k

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1350705-68-8
ethyl (2S,3R)-3-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)-3-hydroxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / Inert atmosphere

2.1: water / 2 h / 90 °C / Inert atmosphere

3.1: tert-butylhypochlorite; sodium hydroxide / propan-1-ol; water / 0.08 h / Inert atmosphere

3.2: 2 h / Inert atmosphere

With tert-butylhypochlorite; tetra-(n-butyl)ammonium iodide; potassium carbonate; sodium hydroxide; In propan-1-ol; water;
DOI:10.1039/c1ob06320k