2-((S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionyl)-nonanoic acid allyl ester

Base Information

Chemical Name:2-((S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionyl)-nonanoic acid allyl ester
CAS No.:1027954-87-5
Molecular Formula:C₃₀H₃₉NO₆
Molecular Weight:509.643
Hs Code.:

Synonyms:2-((S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionyl)-nonanoic acid allyl ester

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Chemical Property of 2-((S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionyl)-nonanoic acid allyl ester

Chemical Property:

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Technology Process of 2-((S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionyl)-nonanoic acid allyl ester

There total 3 articles about 2-((S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionyl)-nonanoic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156631-29-7
heptyl trifluoromethanesulfonate

: 387866-60-6
5-benzyloxy-4(S)-benzyloxycarbonylamino-3-oxopentanoic acid allyl ester

: 1027954-87-5
2-((S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionyl)-nonanoic acid allyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jo010270f

Reference yield:

: 591-87-7
Allyl acetate

: 1027954-87-5
2-((S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionyl)-nonanoic acid allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / carbonyl-1,1'-diimidazole; BuLi; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

2: NaH / tetrahydrofuran / 0 - 20 °C

With n-butyllithium; sodium hydride; diisopropylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran;
DOI:10.1021/jo010270f

Reference yield:

: 20806-43-3
Z-Ser(Bzl)-OH

: 1027954-87-5
2-((S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionyl)-nonanoic acid allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / carbonyl-1,1'-diimidazole; BuLi; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

2: NaH / tetrahydrofuran / 0 - 20 °C

With n-butyllithium; sodium hydride; diisopropylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran;
DOI:10.1021/jo010270f