4-vinylbenzyl methoxypentakis(oxyethylene) ether

Base Information

• Chemical Name: 4-vinylbenzyl methoxypentakis(oxyethylene) ether
• CAS No.: 870809-06-6
• Molecular Formula: C₂₀H₃₂O₆
• Molecular Weight: 368.47
• Mol file: 870809-06-6.mol

Synonyms:4-vinylbenzyl methoxypentakis(oxyethylene) ether

Chemical Property of 4-vinylbenzyl methoxypentakis(oxyethylene) ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-vinylbenzyl methoxypentakis(oxyethylene) ether

There total 3 articles about 4-vinylbenzyl methoxypentakis(oxyethylene) ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

3,6,9,12,15-pentaoxahexadecanol (23778-52-1,95507-80-5) + 4-Vinylbenzyl chloride (1592-20-7,29296-32-0) → 4-vinylbenzyl methoxypentakis(oxyethylene) ether (870809-06-6)

Guidance literature:

3,6,9,12,15-pentaoxahexadecanol; With sodium hydride; In tetrahydrofuran; at 20 ℃;

4-Vinylbenzyl chloride; In tetrahydrofuran; Further stages.; Heating;

DOI:10.1021/ma0514572

Reference yield:

triethylene glucol monomethyl ether (112-35-6,95507-80-5) → 4-vinylbenzyl methoxypentakis(oxyethylene) ether (870809-06-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: NaOH / H₂O; tetrahydrofuran / 0 °C

2.1: Na / 100 °C

2.2: 100 °C

3.1: NaH / tetrahydrofuran / 20 °C

3.2: 35 percent / tetrahydrofuran / Heating

With sodium hydroxide; sodium; sodium hydride; In tetrahydrofuran; water;

DOI:10.1021/ma0514572

Reference yield:

2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate (62921-74-8,518012-62-9,58320-73-3) → 4-vinylbenzyl methoxypentakis(oxyethylene) ether (870809-06-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Na / 100 °C

1.2: 100 °C

2.1: NaH / tetrahydrofuran / 20 °C

2.2: 35 percent / tetrahydrofuran / Heating

With sodium; sodium hydride; In tetrahydrofuran;

DOI:10.1021/ma0514572

upstream raw materials:

3,6,9,12,15-pentaoxahexadecanol

4-Vinylbenzyl chloride

triethylene glucol monomethyl ether

2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate

Refernces