1-Naphthalenemethanol,decahydro-2-hydroxy-5,5,8a-trimethyl-,(1S,2S,4aS,8aR)-(9CI)

Base Information

• Chemical Name: 1-Naphthalenemethanol,decahydro-2-hydroxy-5,5,8a-trimethyl-,(1S,2S,4aS,8aR)-(9CI)
• CAS No.: 807360-95-8
• Molecular Formula: C₁₄H₂₆O₂
• Molecular Weight: 226.359
• Mol file: 807360-95-8.mol

Synonyms:1-Naphthalenemethanol,decahydro-2-hydroxy-5,5,8a-trimethyl-,(1S,2S,4aS,8aR)-(9CI)

Chemical Property of 1-Naphthalenemethanol,decahydro-2-hydroxy-5,5,8a-trimethyl-,(1S,2S,4aS,8aR)-(9CI)

Chemical Property:

• PSA: 40.46000
• LogP: 2.58220

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Naphthalenemethanol,decahydro-2-hydroxy-5,5,8a-trimethyl-,(1S,2S,4aS,8aR)-(9CI)

There total 75 articles about 1-Naphthalenemethanol,decahydro-2-hydroxy-5,5,8a-trimethyl-,(1S,2S,4aS,8aR)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(+/-)-methyl (1α,2β,4aα,8aβ)-2-hydroxy-decahydro-5,5,8a-trimethylnaphthalene-1-carboxylate (65754-79-2,97914-95-9,108774-29-4,108888-65-9,108944-85-0,108944-86-1) → (1α,2β,4aα,8aβ)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol (59633-91-9,65754-93-0,108944-87-2,108944-88-3,136982-34-8,146611-16-7,807360-95-8)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 0.5h;

DOI:10.1248/cpb.48.1176

Reference yield: 98.0%

(+/-)-methyl (1β,2α,4aα,8aβ)-2-formyloxy-decahydro-5,5,8a-trimethylnaphthalene-1-carboxylate (65754-92-9,97914-94-8) → rac-12-nor-drimane-8α,11-diol (59633-91-9,65754-93-0,108944-87-2,108944-88-3,136982-34-8,146611-16-7,807360-95-8)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 4h; Ambient temperature;

DOI:10.1248/cpb.45.824

Reference yield: 97.0%

(+/-)-8-oxo-12-nordriman-11-acid methyl ester (59684-77-4,65794-68-5,115304-46-6,131831-72-6,133102-26-8,49749-46-4,141317-75-1) → 8ξ-hydroxy-9β-hydroxymethyl-(4α,4β),10β-trimethyl-(trans)-decahydronaphthalene (59633-91-9,807360-95-8)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 3h;

DOI:10.1021/jo00211a030

upstream raw materials:

(+/-)-methyl (1α,2α,4aα,8aβ)-2-hydroxy-decahydro-5,5,8a-trimethylnaphthalene-1-carboxylate

methyl 3-oxo-7,11-dimethyl-dodeca-6,10-dienoate

1-methoxycarbonyl-2-oxo-1β,2,3,4,4aα,5,6,7,8aβ-octahydro-5,5,8a-trimethylnaphthalene

(+/-)-methyl (1α,2β,4aα,8aβ)-2-hydroxy-decahydro-5,5,8a-trimethylnaphthalene-1-carboxylate

Downstream raw materials:

(1R,2S,4aR,8aR)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol

(-)-(1S,2R,4aS,8aS)-2-hydroxy-decahydro-5,5,8a-trimethyl-1-naphthylmethanol

(1S,2S,4aS,8aS)-(-)-1-hydroxymethyl 2-hydroxy-5,5,8a-trimethyldecahydronaphthalene

(1R,2R,4aR,8aR)-(-)-1-hydroxymethyl-2-hydroxy-5,5,8a-trimethyldecahydronaphthalene

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