5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine

Base Information

Chemical Name:5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine
CAS No.:1262860-33-2
Molecular Formula:C₁₂H₁₂BrF₃N₂O
Molecular Weight:337.139
Hs Code.:

Synonyms:5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine

Suppliers and Price of 5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine

Chemical Property:

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Technology Process of 5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine

There total 13 articles about 5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1262860-32-1
5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepane-3-thione

: 1262860-33-2
5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine

Guidance literature:: With ammonia; In methanol; for 24h;

Reference yield:

: NH₃/MeOH

: 1262860-32-1
5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepane-3-thione

: 1262860-33-2
5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine

Guidance literature:: With ammonia; In methanol; chloroform;

Reference yield:

: 1262860-22-9
ethyl 3-(5-bromo-2-fluorophenyl)-2,2-difluoro-3-hydroxypropanoate

: 1262860-33-2
5-(5-bromo-2-fluorophenyl)-6,6-difluoro-5-methyl-1,4-oxazepan-3-imine

Guidance literature:: Multi-step reaction with 10 steps

1: ammonium chloride; sodium tetrahydroborate / ethyl acetate; hexane; methanol

2: 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran

3: dichloromethane; ethyl acetate; hexane

4: ethyl acetate; hexane; tetrahydrofuran

5: ammonium chloride / ethyl acetate; hexane; diethyl ether

6: ethyl acetate; hexane; methanol

7: water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran

8: hydrogenchloride; potassium tert-butylate / ethyl acetate; tert-butyl alcohol

9: ethyl acetate; hexane; tetrahydrofuran

10: ammonia / chloroform; methanol

With hydrogenchloride; sodium tetrahydroborate; ammonium chloride; potassium tert-butylate; ammonia; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; chloroform; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; ethyl acetate; tert-butyl alcohol;