dimethyl 2-(3,4-dichlorophenyl)-2-{2-[(methylsulfonyl)oxy]ethyl}-1,1-cyclopropanedicarboxylate

Base Information

Chemical Name:dimethyl 2-(3,4-dichlorophenyl)-2-{2-[(methylsulfonyl)oxy]ethyl}-1,1-cyclopropanedicarboxylate
CAS No.:1013097-84-1
Molecular Formula:C₁₆H₁₈Cl₂O₇S
Molecular Weight:425.287
Hs Code.:

Synonyms:dimethyl 2-(3,4-dichlorophenyl)-2-{2-[(methylsulfonyl)oxy]ethyl}-1,1-cyclopropanedicarboxylate

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Chemical Property of dimethyl 2-(3,4-dichlorophenyl)-2-{2-[(methylsulfonyl)oxy]ethyl}-1,1-cyclopropanedicarboxylate

Chemical Property:

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Technology Process of dimethyl 2-(3,4-dichlorophenyl)-2-{2-[(methylsulfonyl)oxy]ethyl}-1,1-cyclopropanedicarboxylate

There total 3 articles about dimethyl 2-(3,4-dichlorophenyl)-2-{2-[(methylsulfonyl)oxy]ethyl}-1,1-cyclopropanedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1013097-83-0
3-(3,4-dichlorophenyl)-3-buten-1-yl methanesulfonate

: 6773-29-1
dimethyl diazomalonate

: 1013097-84-1
dimethyl 2-(3,4-dichlorophenyl)-2-{2-[(methylsulfonyl)oxy]ethyl}-1,1-cyclopropanedicarboxylate

Guidance literature:: rhodium(II) acetate dimer; In chlorobenzene; at 65 - 67 ℃; for 2.5h; Product distribution / selectivity;

Reference yield:

: 151169-75-4
3,4-dichlophenylboronic acid

: 1013097-84-1
dimethyl 2-(3,4-dichlorophenyl)-2-{2-[(methylsulfonyl)oxy]ethyl}-1,1-cyclopropanedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; water; toluene

2: triethylamine / dichloromethane / 5 - 20 °C / Ice bath

3: dirhodium(II) tetracarboxylate / chlorobenzene / 2.5 h / 65 - 67 °C

With sodium carbonate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dirhodium(II) tetracarboxylate; In ethanol; dichloromethane; water; chlorobenzene; toluene;

Reference yield:

: 272775-65-2
3-(3',4'-dichlorophenyl)-3-buten-1-ol

: 1013097-84-1
dimethyl 2-(3,4-dichlorophenyl)-2-{2-[(methylsulfonyl)oxy]ethyl}-1,1-cyclopropanedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 5 - 20 °C / Ice bath

2: dirhodium(II) tetracarboxylate / chlorobenzene / 2.5 h / 65 - 67 °C

With triethylamine; dirhodium(II) tetracarboxylate; In dichloromethane; chlorobenzene;