(Z)-3-<(dimethylphenylsilyl)methylene>-5-ethyl-2,2-dimethyl-1,2-oxasilolane

Base Information

Chemical Name:(Z)-3-<(dimethylphenylsilyl)methylene>-5-ethyl-2,2-dimethyl-1,2-oxasilolane
CAS No.:151370-57-9
Molecular Formula:C₁₆H₂₆OSi₂
Molecular Weight:290.553
Hs Code.:

Synonyms:(Z)-3-<(dimethylphenylsilyl)methylene>-5-ethyl-2,2-dimethyl-1,2-oxasilolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3-<(dimethylphenylsilyl)methylene>-5-ethyl-2,2-dimethyl-1,2-oxasilolane

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Technology Process of (Z)-3-<(dimethylphenylsilyl)methylene>-5-ethyl-2,2-dimethyl-1,2-oxasilolane

There total 3 articles about (Z)-3-<(dimethylphenylsilyl)methylene>-5-ethyl-2,2-dimethyl-1,2-oxasilolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 151370-43-3
C₁₆H₂₆OSi₂

: 151370-57-9
(Z)-3-<(dimethylphenylsilyl)methylene>-5-ethyl-2,2-dimethyl-1,2-oxasilolane

Guidance literature:: With palladium diacetate; 1,1,3,3-tetramethylbutane isonitrile; In toluene; at 60 ℃; for 13h;
DOI:10.1016/S0040-4020(01)89908-7

Reference yield:

: 19780-84-8
5-Hexyn-3-ol

: 151370-57-9
(Z)-3-<(dimethylphenylsilyl)methylene>-5-ethyl-2,2-dimethyl-1,2-oxasilolane

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, 4-(dimethylamino)pyridine / tetrahydrofuran / Ambient temperature

2: 96 percent / 1,1,3,3-tetramethylbutyl isocyanide, Pd(OAc)2 / toluene / 13 h / 60 °C

With dmap; palladium diacetate; 1,1,3,3-tetramethylbutane isonitrile; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(01)89908-7

Reference yield:

: 941-15-1
1-chloro-2-phenyltetramethyldisilane

: 151370-57-9
(Z)-3-<(dimethylphenylsilyl)methylene>-5-ethyl-2,2-dimethyl-1,2-oxasilolane

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, 4-(dimethylamino)pyridine / tetrahydrofuran / Ambient temperature

2: 96 percent / 1,1,3,3-tetramethylbutyl isocyanide, Pd(OAc)2 / toluene / 13 h / 60 °C

With dmap; palladium diacetate; 1,1,3,3-tetramethylbutane isonitrile; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/S0040-4020(01)89908-7