C₂₅H₃₄F₂N₄OSi

Base Information

Chemical Name:C₂₅H₃₄F₂N₄OSi
CAS No.:1274887-37-4
Molecular Formula:C₂₅H₃₄F₂N₄OSi
Molecular Weight:472.653
Hs Code.:

C<sub>25</sub>H<sub>34</sub>F<sub>2</sub>N<sub>4</sub>OSi

Synonyms:C₂₅H₃₄F₂N₄OSi

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Chemical Property of C₂₅H₃₄F₂N₄OSi

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Technology Process of C₂₅H₃₄F₂N₄OSi

There total 9 articles about C₂₅H₃₄F₂N₄OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1274887-35-2
C₂₅H₃₆F₂N₄OSi

: 1274887-37-4
C₂₅H₃₄F₂N₄OSi

Guidance literature:: With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 42558-50-9,56009-31-5,60793-22-8,133098-13-2
methyl (3R)-3-hydroxypentanoate

: 1274887-37-4
C₂₅H₃₄F₂N₄OSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: dmap; 1H-imidazole / N,N-dimethyl-formamide / 0 °C

1.2: 20 °C

2.1: lithium borohydride / tetrahydrofuran / 2.08 h / 20 °C / Reflux

2.2: 0.5 h / 0 °C

3.1: 4-methylmorpholine N-oxide / dichloromethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

3.2: 1 h

4.1: sodium hydride / n-heptane; tetrahydrofuran / 0.25 h / 0 - 5 °C / Inert atmosphere

4.2: 0 - 20 °C

5.1: ethanol; sodium / 20 °C / Inert atmosphere; Reflux

5.2: 20 - 50 °C

6.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / tetrahydrofuran / 2 h / 110 °C / Microwave irradiation

7.1: manganese(IV) oxide / dichloromethane / 2 h / 20 °C

With 1H-imidazole; dmap; manganese(IV) oxide; lithium borohydride; ethanol; sodium; sodium hydride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 4-methylmorpholine N-oxide; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; n-heptane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 109346-75-0
(3R)-3-(tert-butyldimethylsilyloxy)pentanal

: 1274887-37-4
C₂₅H₃₄F₂N₄OSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / n-heptane; tetrahydrofuran / 0.25 h / 0 - 5 °C / Inert atmosphere

1.2: 0 - 20 °C

2.1: ethanol; sodium / 20 °C / Inert atmosphere; Reflux

2.2: 20 - 50 °C

3.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / tetrahydrofuran / 2 h / 110 °C / Microwave irradiation

4.1: manganese(IV) oxide / dichloromethane / 2 h / 20 °C

With manganese(IV) oxide; ethanol; sodium; sodium hydride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; n-heptane; dichloromethane;