2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutylamine

Base Information

Chemical Name:2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutylamine
CAS No.:144654-00-2
Molecular Formula:C₁₇H₃₅NOSi
Molecular Weight:297.557
Hs Code.:

Synonyms:2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutylamine

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Technology Process of 2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutylamine

There total 2 articles about 2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 144653-99-6
2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile

: 144654-00-2
2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutylamine

Guidance literature:: With diisobutylaluminium hydride; In toluene; at 6 ℃; for 2h;
DOI:10.1016/S0040-4020(01)80461-0

Reference yield:

: 17283-81-7
4-(2,6,6-Trimethyl-cyclohex-1-enyl)-butan-2-on

: 144654-00-2
2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / ZnI₂ / CH₂Cl₂

2: 47 percent / i-Bu₂AlH / toluene / 2 h / 6 °C

With diisobutylaluminium hydride; zinc(II) iodide; In dichloromethane; toluene;
DOI:10.1016/S0040-4020(01)80461-0