2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile

Base Information

Chemical Name:2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile
CAS No.:144653-99-6
Molecular Formula:C₁₇H₃₁NOSi
Molecular Weight:293.525
Hs Code.:

Synonyms:2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile

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Technology Process of 2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile

There total 1 articles about 2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 7677-24-9
trimethylsilyl cyanide

: 17283-81-7
4-(2,6,6-Trimethyl-cyclohex-1-enyl)-butan-2-on

: 144653-99-6
2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile

Guidance literature:: With zinc(II) iodide; In dichloromethane;
DOI:10.1016/S0040-4020(01)80461-0

Reference yield: 47.0%

: 144653-99-6
2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile

: 144654-00-2
2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutylamine

Guidance literature:: With diisobutylaluminium hydride; In toluene; at 6 ℃; for 2h;
DOI:10.1016/S0040-4020(01)80461-0

Reference yield:

: 144653-99-6
2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyronitrile

: 144654-01-3
2-Methyl-4-(2',2',6'-trimethylcyclohex-1'-enyl)-2-trimethylsilyloxybutyraldehyde

Guidance literature:: With sulfuric acid; diisobutylaluminium hydride; ammonium chloride; Yield given. Multistep reaction; 1) a) -45 to 0 deg C, 0.5 h, b) 0 deg C, 1 h, 2) ether, 12 h, r.t.;
DOI:10.1016/S0040-4020(01)80461-0