2-(tetrahydro-2H-pyran-2-yloxy)ethoxycarbonyl(phenyl)methyl dithiobenzoate

Base Information

• Chemical Name: 2-(tetrahydro-2H-pyran-2-yloxy)ethoxycarbonyl(phenyl)methyl dithiobenzoate
• CAS No.: 1238539-04-2
• Molecular Formula: C₂₂H₂₄O₄S₂
• Molecular Weight: 416.562

Synonyms:2-(tetrahydro-2H-pyran-2-yloxy)ethoxycarbonyl(phenyl)methyl dithiobenzoate

Chemical Property of 2-(tetrahydro-2H-pyran-2-yloxy)ethoxycarbonyl(phenyl)methyl dithiobenzoate

Chemical Property:

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Technology Process of 2-(tetrahydro-2H-pyran-2-yloxy)ethoxycarbonyl(phenyl)methyl dithiobenzoate

There total 1 articles about 2-(tetrahydro-2H-pyran-2-yloxy)ethoxycarbonyl(phenyl)methyl dithiobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

carbon disulfide (75-15-0,12122-00-8) + 2-(tetrahydro-2H-pyran-2-yloxy)ethyl α-bromophenylacetate (1238539-02-0) + phenylmagnesium bromide (100-58-3) → 2-(tetrahydro-2H-pyran-2-yloxy)ethoxycarbonyl(phenyl)methyl dithiobenzoate (1238539-04-2)

Guidance literature:

carbon disulfide; phenylmagnesium bromide; In tetrahydrofuran; at 0 ℃; for 4h; Inert atmosphere;

2-(tetrahydro-2H-pyran-2-yloxy)ethyl α-bromophenylacetate; In tetrahydrofuran; at 85 ℃; for 24h; Inert atmosphere;

DOI:10.1002/pola.24082

Reference yield: 65.0%

2-(tetrahydro-2H-pyran-2-yloxy)ethoxycarbonyl(phenyl)methyl dithiobenzoate (1238539-04-2) → 2-hydroxyethoxycarbonyl(phenyl)methyl dithiobenzoate (1238539-05-3)

Guidance literature:

With copper(ll) sulfate pentahydrate; In methanol; at 20 ℃; for 12h;

DOI:10.1002/pola.24082

upstream raw materials:

carbon disulfide

2-(tetrahydro-2H-pyran-2-yloxy)ethyl α-bromophenylacetate

phenylmagnesium bromide

Downstream raw materials:

2-hydroxyethoxycarbonyl(phenyl)methyl dithiobenzoate

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