3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione

Base Information

Chemical Name:3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione
CAS No.:1225448-23-6
Molecular Formula:C₁₇H₁₅BrN₂O₂S
Molecular Weight:391.288
Hs Code.:

Synonyms:3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione

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Chemical Property of 3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione

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Technology Process of 3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione

There total 2 articles about 3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18791-78-1
4-bromothiophene-3-carboxaldehyde

: 1208118-33-5
1,4-diacetyl-3-benzyl-3-methylpiperazine-2,5-dione

: 1225448-23-6
3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 14 h / 20 - 25 °C

2: hydrazine hydrate / N,N-dimethyl-formamide / 20 - 25 °C

With potassium carbonate; hydrazine hydrate; In N,N-dimethyl-formamide; 1: Aldol Condensation;

Reference yield:

: 1225448-22-5
1-Acetyl-6-benzyl-3-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-6-methyl-piperazine-2,5-dione

: 1225448-23-6
3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione

Guidance literature:: With hydrazine hydrate; In N,N-dimethyl-formamide; at 20 - 25 ℃;

Reference yield:

: 1225448-23-6
3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione

: 74-88-4
methyl iodide

: 1225446-84-3
3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-1,3,4-trimethyl-piperazine-2,5-dione

Guidance literature:: 3-Benzyl-6-[1-(4-bromothiophen-3-yl)meth-(Z)-ylidene]-3-methylpiperazine-2,5-dione; With sodium hydride; In paraffin oil (nujol); N,N-dimethyl-formamide; at 0 ℃; for 2h;

methyl iodide; In paraffin oil (nujol); N,N-dimethyl-formamide; at 0 - 25 ℃; for 14h;