Technology Process of C37H44O5
There total 5 articles about C37H44O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Crabtree's catalyst; hydrogen;
In
dichloromethane;
at 20 ℃;
for 48h;
Inert atmosphere;
DOI:10.1248/cpb.60.137
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: toluene / 5 h / 120 °C / Inert atmosphere
3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere
3.2: -78 °C / Inert atmosphere
4.1: Crabtree's catalyst; hydrogen / dichloromethane / 48 h / 20 °C / Inert atmosphere
With
n-butyllithium; Crabtree's catalyst; hydrogen; sodium hexamethyldisilazane;
In
tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1248/cpb.60.137
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: toluene / 5 h / 120 °C / Inert atmosphere
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere
2.2: -78 °C / Inert atmosphere
3.1: Crabtree's catalyst; hydrogen / dichloromethane / 48 h / 20 °C / Inert atmosphere
With
Crabtree's catalyst; hydrogen; sodium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1248/cpb.60.137
