3-Chlor-10-<3-(dimethylamino)propyl>-9,9-dimethyl-9-silaacridan

Base Information

• Chemical Name: 3-Chlor-10-<3-(dimethylamino)propyl>-9,9-dimethyl-9-silaacridan
• CAS No.: 79369-97-4
• Molecular Formula: C₁₉H₂₅ClN₂Si
• Molecular Weight: 344.959

Synonyms:3-Chlor-10-<3-(dimethylamino)propyl>-9,9-dimethyl-9-silaacridan

Chemical Property of 3-Chlor-10-<3-(dimethylamino)propyl>-9,9-dimethyl-9-silaacridan

Chemical Property:

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Technology Process of 3-Chlor-10-<3-(dimethylamino)propyl>-9,9-dimethyl-9-silaacridan

There total 1 articles about 3-Chlor-10-<3-(dimethylamino)propyl>-9,9-dimethyl-9-silaacridan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-5-chloroaniline (823-57-4) → 3-Chlor-10-<3-(dimethylamino)propyl>-9,9-dimethyl-9-silaacridan (79369-97-4)

Guidance literature:

Multi-step reaction with 7 steps

1: 93 percent / N,N-Dimethylaniline / 0.75 h / 100 °C

2: 87 percent / PCl₅ / 1) 3 h, room temperature, 2) 1 h, 100 deg C

3: 78 percent / NaOEt / diethyl ether / 1) 4 h, 0 deg C, 2) 12 h, room temperature

4: 40 percent / 1) 150 min, 257-260 deg C, 2) 40 deg C, 3) ethanol, 0 deg C

5: 86 percent / KOH / ethanol; H₂O / 40 h / Heating

6: 1) NaNH₂ / 1) benzene, toluene, 1 h, 80 deg C, 2) toluene, 18 h, reflux

7: 1) BuLi (15percent n-hexane) / acetone / 1) ether, 1 h, 0 deg C, 2) ether, 15 h, 20 deg C; 1 h, reflux

With potassium hydroxide; n-butyllithium; phosphorus pentachloride; sodium ethanolate; sodium amide; N,N-dimethyl-aniline; In diethyl ether; ethanol; water; acetone;

DOI:10.1002/jlac.198119810715

upstream raw materials:

2-bromo-5-chloroaniline

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