C₂₄H₃₂O₄S

Base Information

• Chemical Name: C₂₄H₃₂O₄S
• CAS No.: 1262416-86-3
• Molecular Formula: C₂₄H₃₂O₄S
• Molecular Weight: 416.582
• Mol file: 1262416-86-3.mol

Synonyms:C₂₄H₃₂O₄S

Chemical Property of C₂₄H₃₂O₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₂O₄S

There total 6 articles about C₂₄H₃₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C21H28O4S (1262416-70-5) + 2,2-dimethoxy-propane (77-76-9) → C24H32O4S (1262416-86-3)

Guidance literature:

With CSA; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/jo1019909

Reference yield:

C20H22O3S → C24H32O4S (1262416-86-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: zinc(II) chloride / tetrahydrofuran / 0.5 h / 20 °C

1.2: 1 h / -78 °C / Inert atmosphere

1.3: 20 °C / pH 2

2.1: diethylzinc / 1,2-dimethoxyethane; hexane; dichloromethane / 0.92 h / 0 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere; Cooling

3.1: water; mercury(II) trifluoroacetate; mercury(II) oxide / 1,2-dichloro-ethane / 16 h / 20 °C / Inert atmosphere; Darkness

4.1: CSA / dichloromethane / 3 h / 20 °C

With water; diethylzinc; mercury(II) trifluoroacetate; mercury(II) oxide; zinc(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; dichloromethane; 1,2-dichloro-ethane;

DOI:10.1021/jo1019909

Reference yield:

C20H24O3S → C24H32O4S (1262416-86-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: diethylzinc / 1,2-dimethoxyethane; hexane; dichloromethane / 0.92 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere; Cooling

2.1: water; mercury(II) trifluoroacetate; mercury(II) oxide / 1,2-dichloro-ethane / 16 h / 20 °C / Inert atmosphere; Darkness

3.1: CSA / dichloromethane / 3 h / 20 °C

With water; diethylzinc; mercury(II) trifluoroacetate; mercury(II) oxide; In 1,2-dimethoxyethane; hexane; dichloromethane; 1,2-dichloro-ethane;

DOI:10.1021/jo1019909

upstream raw materials:

C₂₁H₂₆O₃S

C₂₁H₂₈O₄S

2,2-dimethoxy-propane

3-benzyloxypropanone