bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate)

Base Information

Chemical Name:bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate)
CAS No.:1260632-53-8
Molecular Formula:C₇₆H₁₁₄N₆O₁₄
Molecular Weight:1335.77
Hs Code.:

bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate)

Synonyms:bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate)

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Chemical Property of bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate)

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Technology Process of bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate)

There total 14 articles about bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1260632-36-7
2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate

: 1260632-26-5
3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarboxylic acid

: 1260632-53-8
bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate)

Guidance literature:: 3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarboxylic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 4h; Inert atmosphere;

2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate; In dichloromethane; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1021/ol102522m

Reference yield:

: C₃₀H₄₄O₆

: 1260632-53-8
bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; sodium hydroxide / methanol / 20 °C

2.1: water; sodium hydroxide / methanol / 4 h / Reflux

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / Inert atmosphere

3.2: 36 h / 20 °C / Inert atmosphere

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1021/ol102522m

Reference yield:

: 1260632-34-5
2-(isopentyloxy)ethyl-3-amino-5-(2-ethylhexanamido)benzoate

: 1260632-53-8
bis(2-(isopentyloxy)ethyl)-5,5'-((2,2'-((3,6-bis((2-ethylhexyl)oxy)naphthalene-2,7-dicarbonyl)bis(azanediyl))bis(acetyl))bis(azanediyl))bis(3-(2-ethylhexanamido)benzoate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C

1.2: 24 h / Darkness

2.1: trifluoroacetic acid / dichloromethane / 3 h

3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / Inert atmosphere

3.2: 36 h / 20 °C / Inert atmosphere

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ol102522m