2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate

Base Information

Chemical Name:2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate
CAS No.:1260632-36-7
Molecular Formula:C₂₄H₃₉N₃O₅
Molecular Weight:449.591
Hs Code.:

Synonyms:2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate

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Chemical Property of 2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate

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Technology Process of 2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate

There total 7 articles about 2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: C₂₇H₄₃N₃O₆

: 1260632-36-7
2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 3h;
DOI:10.1021/ol102522m

Reference yield:

: C₂₀H₃₀N₂O₅

: 1260632-36-7
2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 10% palladium on activated charcoal; hydrogen / dichloromethane

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C

2.2: 24 h / Darkness

3.1: trifluoroacetic acid / dichloromethane / 3 h

With 10% palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ol102522m

Reference yield:

: 1260632-29-8
2-(isopentyloxy)ethyl-3,5-dinitrobenzoate

: 1260632-36-7
2-(isopentyloxy)ethyl-3-(2-aminoacetamido)-5-(2-ethylhexanamido)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: iron; acetic acid / 2 h / Cooling with ice

2.1: triethylamine / dichloromethane / 12 h / Reflux

3.1: 10% palladium on activated charcoal; hydrogen / dichloromethane

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C

4.2: 24 h / Darkness

5.1: trifluoroacetic acid / dichloromethane / 3 h

With 10% palladium on activated charcoal; hydrogen; iron; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ol102522m