1,1-dimethylethyl-4-[(3,4-dichlorophenyl)carbonyl]-1-piperidinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl-4-[(3,4-dichlorophenyl)carbonyl]-1-piperidinecarboxylate
CAS No.:269731-79-5
Molecular Formula:C₁₇H₂₁Cl₂NO₃
Molecular Weight:358.265
Hs Code.:

Synonyms:1,1-dimethylethyl-4-[(3,4-dichlorophenyl)carbonyl]-1-piperidinecarboxylate

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Chemical Property of 1,1-dimethylethyl-4-[(3,4-dichlorophenyl)carbonyl]-1-piperidinecarboxylate

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Technology Process of 1,1-dimethylethyl-4-[(3,4-dichlorophenyl)carbonyl]-1-piperidinecarboxylate

There total 4 articles about 1,1-dimethylethyl-4-[(3,4-dichlorophenyl)carbonyl]-1-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 269731-79-5
1,1-dimethylethyl-4-[(3,4-dichlorophenyl)carbonyl]-1-piperidinecarboxylate

Guidance literature:: With iodine; magnesium; In tetrahydrofuran; at 60 ℃; for 1h; Inert atmosphere;

In tetrahydrofuran; at 0 - 30 ℃; for 3h; Inert atmosphere;

Reference yield:

: 220772-30-5
1-(tert-butoxycarbonyl)-4-(3,4-dichloro-benzylidene)piperidine

: 269731-79-5
1,1-dimethylethyl-4-[(3,4-dichlorophenyl)carbonyl]-1-piperidinecarboxylate

Guidance literature:: 1-(tert-butoxycarbonyl)-4-(3,4-dichloro-benzylidene)piperidine; With borane-THF; In tetrahydrofuran; at 20 ℃; for 3h;

With water;

With sodium dichromate; sulfuric acid; In water; at 20 ℃; for 2h;