1,1-dimethylethyl-4-[(3,4-dichlorophenyl)(hydroxy)methyl]-1-piperidinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl-4-[(3,4-dichlorophenyl)(hydroxy)methyl]-1-piperidinecarboxylate
CAS No.:645379-16-4
Molecular Formula:C₁₇H₂₃Cl₂NO₃
Molecular Weight:360.281
Hs Code.:

Synonyms:1,1-dimethylethyl-4-[(3,4-dichlorophenyl)(hydroxy)methyl]-1-piperidinecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-dimethylethyl-4-[(3,4-dichlorophenyl)(hydroxy)methyl]-1-piperidinecarboxylate

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Technology Process of 1,1-dimethylethyl-4-[(3,4-dichlorophenyl)(hydroxy)methyl]-1-piperidinecarboxylate

There total 2 articles about 1,1-dimethylethyl-4-[(3,4-dichlorophenyl)(hydroxy)methyl]-1-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.7%

: 645379-16-4
1,1-dimethylethyl-4-[(3,4-dichlorophenyl)(hydroxy)methyl]-1-piperidinecarboxylate

Guidance literature:: With methanol; sodium tetrahydroborate; at 20 ℃; for 1h;

Reference yield:

: 18282-59-2
4-bromo-1,2-dichlorobenzene

: 137076-22-3
tert butyl 4-formylpiperidine-1-carboxylate

: 645379-16-4
1,1-dimethylethyl-4-[(3,4-dichlorophenyl)(hydroxy)methyl]-1-piperidinecarboxylate

Guidance literature:: 4-bromo-1,2-dichlorobenzene; With iodine; magnesium; In tetrahydrofuran; for 0.5h; Heating / reflux;

tert butyl 4-formylpiperidine-1-carboxylate; In tetrahydrofuran; at 0 - 23 ℃; for 0.75h;